Chrome-Free Polyurethane-Silicon Oxide Metal Surface Treatment

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Solution Overview

Problem

Current hexavalent chrome-free surface treatments for steel sheets lack sufficient corrosion resistance, alkali resistance, solvent resistance, and paint adhesion, and often require high temperatures for curing, which complicates industrial application.

Innovation Solution

A surface treatment agent combining polyurethane resin with silicon oxide, silanol groups, and specific bonding agents to create a crosslinked film structure with optimal ratios of urea and urethane bonds, allowing for improved adhesion, corrosion resistance, and lower curing temperatures.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a chromate treatment is used to provide anti-rust and paint adhesion, then corrosion resistance and paint adhesion are improved, but environmental harm increases due to hexavalent chrome content

Engineering Contradiction:
Improvecorrosion resistanceVSAvoidhexavalent chrome content
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The invention changes the chemical composition parameters by replacing hexavalent chrome with specific combinations of inorganic compounds (phosphate, silicate, sulfate) and organic compounds (urethane resin, carboxylic acid), achieving corrosion resistance without harmful substances

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses composite material approach by combining multiple inorganic compounds with organic compounds to create a surface treatment layer that provides both corrosion resistance and environmental compatibility

Inventive Principle:
Principle #40Composite materials

2Ease of operation

If an organic film is used to substitute chromate treatment, then formability is improved, but adhesion to overcoating paint deteriorates and marks occur during machining

Engineering Contradiction:
ImproveformabilityVSAvoidadhesion to overcoating paint
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The invention combines organic compounds (urethane resin) with inorganic compounds (phosphate, silicate, sulfate) to create a composite surface treatment that maintains formability while providing adequate adhesion to overcoating paint

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention applies different functional components to different aspects of the surface treatment: organic compounds provide formability and base adhesion, while inorganic compounds provide corrosion resistance and enhanced paint adhesion

Inventive Principle:
Principle #3Local quality

3Ease of operation

If the urethane resin structure is not optimized, then film formability is improved, but alkali resistance, workability, and solvent resistance deteriorate

Engineering Contradiction:
Improvefilm formabilityVSAvoidalkali resistance and solvent resistance
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The invention optimizes the chemical structure parameters of the urethane resin by controlling the ratio of hydroxyl groups to isocyanate groups and adjusting the molecular weight and composition to achieve both formability and resistance properties

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite system where the urethane resin structure is combined with inorganic compounds, allowing the organic component to provide formability while the inorganic component enhances resistance to alkali and solvents

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides a hexavalent chrome-free surface treatment with enhanced corrosion resistance, alkali resistance, solvent resistance, and paint adhesion, while allowing for lower temperature processing, making it more industrially viable.

Implementation Method 1

the polyurethane resin contains bond due to siloxane bond, dehydration-condensation bond of silanol group and different functional group

Methodology Applied
Scientific EffectDehydration-condensation reaction: Chemical Bonding

Implementation Method 2

by first obtaining a surface treatment agent by mixing polyurethane resin and silicon oxide... through a stable and good crosslinking reaction

Methodology Applied
Scientific EffectCrosslinking reaction: Chemical Bonding

Data Source

PatentUS8034456B2Surface-treated metal material and metal surface treatment agent
Publication Date: 2011.10.11 MITSUI CHEMICALS INC

AI summary

The present invention provides a surface-treated metal material having a film formed on at least a portion of a surface of a metal material, the film containing at least polyurethane resin and silicon oxide, and a metal surface treatment agent used to obtain the surface-treated metal material. The polyurethane resin contains one or more of siloxane bond, dehydration-condensation bond of silanol group and different functional group, and silanol moiety, and urea bond. The sum of the siloxane bond, the dehydration-condensation bond of silanol group and different functional group, total amount of the silanol moiety, and the silicon oxide falls within a range of equal to or more than 1.6 wt % to equal to or less than 25 wt % for solids of the film. The ratio of the total amount of urea bond and urethane bond to the total amount of resin components falls within a range of equal to or more than 0.1 wt % to equal to or less than 10 wt %.