Porous Free-Standing Thick Electrode Sheet for Flexible Battery Scaling

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Solution Overview

Problem

Existing electrode manufacturing techniques for rechargeable batteries face challenges in producing flexible, porous, and self-supporting thick electrodes with uniform microstructure and high mechanical strength, particularly for aqueous hybrid ion batteries, due to issues with porosity, electrical conductivity, and scalability, as well as sensitivity to additives and complexity in the fabrication process.

Innovation Solution

A semi-dry process involving the mixing of ceramic powder and conductive agents with solvents and additives, followed by high-speed shearing and roller pressing to create a uniform dough, which is then dried and refined to produce a flexible, porous, and self-supporting thick electrode sheet with adjustable porosity and conductivity, allowing for large-scale production without the need for complex machinery.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If wet-coating process is used to manufacture electrode, then electrode can be formed with binder and solvent, but drying process is insufficient and residual additives remain in electrode

Engineering Contradiction:
Improveease of manufactureVSAvoidelectrode performance
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent removes the drying step entirely from the manufacturing process by using a self-binding polymer system that cures at room temperature or low temperature, eliminating the need for high-temperature drying that causes residual additive problems

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent changes the binding mechanism from physical adhesion requiring drying to chemical cross-linking that occurs at low temperatures, fundamentally altering the process parameters to avoid residual additive issues

Inventive Principle:
Principle #35Parameter changes

2Loss of time

If dry binder formulations are used to eliminate drying step, then drying process is eliminated, but porosity and mechanical strength of electrode sheet deteriorate

Engineering Contradiction:
Improvetime consumptionVSAvoidmechanical strength
Core Design Contradiction:
Loss of timeVSStrength

Solution Approach 1:

The patent uses a composite polymer system combining self-binding polymer with cross-linking agents to achieve both mechanical strength and porosity without requiring drying, creating a material that simultaneously satisfies multiple requirements

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent creates a porous electrode structure through the polymer cross-linking process itself, where the cross-linked polymer network forms the porous framework that provides both mechanical strength and ion transport pathways

Inventive Principle:
Principle #31Porous materials

3Manufacturing precision

If wet-coating process is used to manufacture thin electrode, then electrode can be coated onto substrate, but electrode is not self-supporting and requires current collector

Engineering Contradiction:
Improvethickness controlVSAvoidstructure complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent creates a self-supporting electrode structure where the cross-linked polymer network provides inherent mechanical strength, allowing the electrode to stand alone without requiring a separate current collector substrate

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The patent combines active material particles with cross-linked polymer to create a composite structure that is both mechanically self-supporting and electrochemically functional

Inventive Principle:
Principle #40Composite materials

4Shape

If additives are introduced during electrode fabrication, then desired microscopic morphology can be obtained, but performance of supercapacitor deteriorates

Engineering Contradiction:
Improvemicroscopic morphologyVSAvoiddevice performance
Core Design Contradiction:
ShapeVSReliability

Solution Approach 1:

The patent removes traditional additives from the formulation and replaces their functional roles with the self-binding polymer and cross-linking system, eliminating harmful substances while maintaining desired morphology

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method results in electrodes with improved flexibility, uniform surface density, high mechanical strength, and enhanced electrochemical performance, enabling the production of aqueous hybrid ion batteries with extended cycle life and reduced environmental impact.

Implementation Method 1

a polymer binder is dissolved in a solvent and cross-linked with the surrounding particles

Methodology Applied
Scientific EffectCross-linking: Chemical Bonding

Implementation Method 2

when subjected to high shear mixing, serves to fibrillate the binder

Methodology Applied
Scientific EffectShear stress: Shear Stress

Implementation Method 3

A continuous free-standing electrode green sheet can be obtained by rolling the dough through a roller press

Methodology Applied
Scientific EffectCompression: Compression

Implementation Method 4

Once solvent is removed, the polymers become sticky and provide adhesion to a substrate or cohesion between particles

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentEP4231371A1A porous free-standing flexible thick electrode sheet and its preparation method
Publication Date: 2023.08.23 ZONKE SENO TECH CO LTD
  • EP4231371A1 patent drawingFigure 1~2
  • EP4231371A1 patent drawingFigure 3~4
  • EP4231371A1 patent drawingFigure 5

AI summary

The present invention provides a porous free-standing flexible thick electrode, its fabrication method, and an aqueous hybrid ion battery made with said electrode. This free-standing flexible thick electrode provides a flexible thick electrode sheet characterized by an active material load of 0.01 - 2 g/cm2, a thickness range from 0.01 - 4 mm, porosity range from 15-60%, tensile strength range from 0.2 - 5 MPa, tensile elongation at break range from 5-25%, volume resistivity range from 0.1 - 10 Ω·cm, tolerance of pH 2-13, a width of 0.01 - 2 m, and an unrestricted length, even tens of meters.