Powder Pretreatment for Additive Manufacturing Grain Control

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Solution Overview

Problem

Additive manufacturing systems, such as DMLM, face challenges in achieving optimal microstructure and mechanical properties due to fine grain sizes and inferior creep resistance in fabricated components, primarily because of the fine arrays of second phase precipitates resulting from rapid cooling of the melt pool.

Innovation Solution

A pretreatment heating system is used to coarsen second phase particles in the powdered feedstock material before additive manufacturing, ensuring these particles persist and influence the grain size of the consolidated component, thereby improving recrystallization and creep behavior by applying controlled heat and energy during the process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Length of moving object

If rapid cooling of the melt pool is used in additive manufacturing, then fine grain sizes are achieved, but recrystallization difficulty and inferior mechanical behavior occur

Engineering Contradiction:
Improvegrain sizeVSAvoidmechanical behavior
Core Design Contradiction:
Length of moving objectVSReliability

Solution Approach 1:

The patent applies preliminary action by pre-coarsening the second phase precipitates in the powder feedstock before the additive manufacturing process. This pre-treatment ensures that when the material is rapidly cooled during printing, the coarsened particles are already present to serve as effective nucleation sites and grain growth promoters, thereby achieving both fine control over grain size and improved mechanical properties including recrystallization behavior.

Inventive Principle:
Principle #10Preliminary action

2Length of moving object

If fine arrays of second phase precipitates are present in the powder material, then fine grain sizes are produced, but creep resistance deteriorates

Engineering Contradiction:
Improvegrain sizeVSAvoidcreep resistance
Core Design Contradiction:
Length of moving objectVSStrength

Solution Approach 1:

The patent applies parameter changes by modifying the size parameter of the second phase precipitates through thermal treatment before additive manufacturing. By heating the powder to specific temperatures and holding it for controlled durations, the precipitates coarsen from fine arrays to larger, more spaced-out structures. This parameter change in precipitate size directly improves creep resistance while maintaining grain size control through the modified particle distribution.

Inventive Principle:
Principle #35Parameter changes

3Strength

If pretreatment heating is applied to coarsen particles, then creep resistance and grain size improve, but process complexity increases

Engineering Contradiction:
Improvecreep resistanceVSAvoidprocess complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent merges the pretreatment heating step with the existing powder preparation and handling infrastructure of the additive manufacturing system. Rather than adding a completely separate complex system, the heating process is integrated into the powder feedstock preparation workflow, utilizing standard thermal treatment equipment and procedures that can be incorporated into the existing manufacturing flow, thereby minimizing additional complexity while achieving the desired particle coarsening.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method effectively increases grain sizes and enhances recrystallization and creep behavior of the alloy, making it comparable to cast forms, while maintaining the benefits of additive manufacturing in terms of cost and efficiency.

Implementation Method 1

A pretreatment heating system is used to coarsen second phase particles in the powdered feedstock material before additive manufacturing

Methodology Applied
Scientific EffectThermal diffusion: Diffusion

Implementation Method 2

directing an energy beam emitted by an energy device onto a layer of the powdered material, and generating a melt pool in the powdered material layer with the energy beam

Methodology Applied
Scientific EffectLaser heating: Laser

Implementation Method 3

The melt pool cools quickly resulting in fine arrays of second phase precipitates within the fabricated component

Methodology Applied
Scientific EffectRapid cooling: Cooling

Data Source

PatentUS10758976B2Systems and methods for powder pretreatment in additive manufacturing
Publication Date: 2020.09.01 GENERAL ELECTRIC CO
  • US10758976B2 patent drawing
  • US10758976B2 patent drawing
  • US10758976B2 patent drawing

AI summary

A method of processing a powdered feedstock to form a fabricated component is provided. The fabricated component includes a plurality of grains having a nominal grain size. The method includes providing the powdered feedstock material having a population of phase particulates with a first nominal size distribution disposed within a host matrix material. The method includes building a consolidated component from the powdered feedstock material in an additive manufacturing process, and fabricating the fabricated component from the consolidated component. The first nominal size distribution of the population of phase particulates is sized such that at least a portion of the population of phase particulates persists throughout the additive manufacturing process and is present as a processed population of phase particulates in the consolidated component. In addition, the processed population of phase particulates has a second nominal size distribution effective to produce the nominal grain size of the fabricated component.