Precursor Supply Heating Control for Stable Vapor Concentration

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Solution Overview

Problem

Existing gas supply systems for semiconductor and dry coating processes face challenges in maintaining precursor concentration, accurately detecting residual amounts, and efficiently heating vessels due to complex structures, temperature control issues, and fluctuations in precursor supply, leading to inconsistent film formation and unnecessary precursor consumption.

Innovation Solution

A precursor supply system with a vessel heating unit, carrier gas heating unit, and measurement units for controlling temperature and gas flow, ensuring the precursor is supplied at the required concentration and accurately detecting residual amounts by controlling the carrier gas temperature and vessel temperature based on real-time measurements.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If the vessel structure is made complex (e.g., adding trays) to increase precursor supply stability, then the precursor supply stability is improved, but the device complexity and operational difficulty increase

Engineering Contradiction:
Improveprecursor supply stabilityVSAvoidvessel structure complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent extracts the heating function from the vessel structure itself and places it in a separate heating unit. This allows the vessel to remain simple while achieving stable precursor supply through controlled heating, eliminating the need for complex internal structures like trays.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent introduces a heating control unit that monitors and adjusts the heating temperature based on precursor supply conditions. This feedback mechanism ensures stable precursor vaporization and supply without requiring complex vessel structures, as the system dynamically adapts to maintain optimal conditions.

Inventive Principle:
Principle #23Feedback

2Productivity

If the heating temperature is increased to improve precursor vaporization, then the precursor supply amount is improved, but the risk of temperature overshoot and precursor degradation increases

Engineering Contradiction:
Improveprecursor supply amountVSAvoidtemperature control stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent employs dynamic temperature control where the heating unit adjusts its output based on real-time conditions. The heating control unit modulates the heating temperature to match the actual precursor supply needs, preventing both insufficient vaporization and dangerous overshoot conditions.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent changes the heating temperature parameter dynamically rather than maintaining a fixed high temperature. The heating control unit adjusts the temperature parameter based on precursor consumption rate and supply requirements, optimizing both productivity and safety by keeping the temperature within a controlled range.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If the vessel heating time is extended to ensure complete precursor vaporization, then the precursor supply completeness is improved, but the processing time and productivity are reduced

Engineering Contradiction:
Improveprecursor supply completenessVSAvoidprocessing speed
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The patent performs preliminary heating of the vessel and precursor materials before actual precursor supply begins. The heating control unit pre-heats the system to the required temperature, ensuring that when precursor supply starts, vaporization occurs immediately and completely without delays, thus maintaining both completeness and speed.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent maintains continuous heating during the precursor supply process rather than intermittent heating. The heating unit continuously provides thermal energy to ensure complete and consistent precursor vaporization throughout the supply period, eliminating the need for extended heating cycles while maintaining supply completeness.

Inventive Principle:
Principle #20Continuity of useful action

4Productivity

If the carrier gas flow rate is increased to improve precursor entrainment, then the precursor supply efficiency is improved, but the precursor concentration control and waste reduction become more difficult

Engineering Contradiction:
Improveprecursor supply efficiencyVSAvoidprecursor concentration control
Core Design Contradiction:
ProductivityVSMeasurement precision

Solution Approach 1:

The patent introduces a flow control unit that monitors and adjusts the carrier gas flow rate based on precursor supply conditions. This feedback mechanism ensures that the carrier gas flow is optimized to entrain precursor effectively while maintaining the required concentration levels, preventing both insufficient mixing and excessive waste.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent dynamically adjusts the carrier gas flow rate parameter rather than using a fixed high flow rate. The flow control unit modifies the flow rate based on precursor vaporization rate and supply requirements, optimizing the balance between supply efficiency and concentration control, thereby reducing precursor waste while maintaining productivity.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system ensures stable and uniform precursor supply, reducing waste and fluctuations, allowing for precise control of precursor concentration and detection of residual amounts, thereby improving the film formation process and reducing operational costs.

Implementation Method 1

the solid material or liquid material inside the vessel is indirectly heated

Methodology Applied
Scientific EffectSublimation: Sublimation

Implementation Method 2

must be vaporized for supply in the case of liquid materials

Methodology Applied
Scientific EffectVaporization: Evaporation

Implementation Method 3

a carrier gas heating unit which is disposed in the introduction line and heats the carrier gas

Methodology Applied
Scientific EffectHeating: Heating

Data Source

PatentUS11819838B2Precursor supply system and precursors supply method
Publication Date: 2023.11.21 LAIR LIQUIDE SA POUR LETUDE & LEXPLOITATION DES PROCEDES GEORGES CLAUDE
  • US11819838B2 patent drawing
  • US11819838B2 patent drawing
  • US11819838B2 patent drawing

AI summary

The present invention provides a supply system enabling a precursor of a solid material or a precursor of a liquid material to be supplied to a latter process at no higher concentration than required and also at or above a predetermined concentration.A supply system 1 comprises: a vessel 11 for receiving a precursor material; a vessel heating unit for heating the vessel at a set temperature; a carrier gas heating unit which is disposed in an introduction line L1 and heats a carrier gas; a main measurement unit which is disposed in an outward conduction line L2 and obtains data relating to a gas of the precursor; and a carrier gas temperature control unit for controlling the temperature of the carrier gas heating unit in accordance with a measurement result of the main measurement unit.