Pre-heating Substrate for Uniform Ceramic Thermal Barrier Coatings

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Solution Overview

Problem

Conventional Electron Beam Physical Vapor Deposition (EB-PVD) methods for coating gas turbine engine airfoils face challenges in achieving uniform thermal barrier coatings due to premature deposition of ceramic materials before the substrate is adequately heated, which can affect the adhesion and stoichiometry of the final coating.

Innovation Solution

A method involving pre-heating the substrate using an electron beam source to establish a desired evaporation rate of ceramic material, ensuring the substrate reaches an oxidation temperature to form an oxide layer without premature deposition, utilizing controlled gas flow, heating area, and filament current to prevent unwanted evaporation during the pre-heating stage, followed by precise deposition of the ceramic thermal barrier coating.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If the electron beam source is used to heat the ceramic material before deposition, then the substrate reaches oxidation temperature to form an oxide layer, but the ceramic material may evaporate prematurely and deposit onto the substrate before appropriate heating

Engineering Contradiction:
Improvesubstrate temperatureVSAvoidcoating uniformity
Core Design Contradiction:
TemperatureVSManufacturing precision

Solution Approach 1:

The electron beam source is used to pre-heat the substrate to oxidation temperature before ceramic material deposition begins. This preliminary heating action ensures the substrate reaches the required temperature for oxide layer formation, preventing premature deposition and ensuring coating uniformity. The system performs the heating action in advance, before the main deposition process starts.

Inventive Principle:
Principle #10Preliminary action

2Productivity

If the heating rate is increased to reach oxidation temperature quickly, then productivity improves, but the ceramic material evaporates prematurely affecting coating quality

Engineering Contradiction:
Improvecoating process speedVSAvoidcoating stoichiometry
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The system performs preliminary heating of the substrate to oxidation temperature before initiating ceramic material deposition. This advance preparation ensures that when deposition starts, the substrate is already at the correct temperature, preventing premature evaporation and maintaining proper coating stoichiometry while allowing for efficient process timing.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The system monitors the heating process and ceramic material evaporation rate, adjusting parameters to maintain optimal conditions. Feedback control ensures that the substrate reaches oxidation temperature without causing premature ceramic material evaporation, balancing productivity with coating quality and stoichiometry control.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances the adhesion and uniformity of the ceramic thermal barrier coating by ensuring the substrate is properly oxidized before coating, maintaining the stoichiometry and preventing unwanted deposition during the pre-heating stage, thereby improving the overall coating process efficiency.

Implementation Method 1

an electron beam source is used to heat a ceramic material within the coating chamber

Methodology Applied
Scientific EffectElectron beam heating: Electron Beam

Implementation Method 2

The ceramic material radiates heat that heats the substrate to an oxidation temperature

Methodology Applied
Scientific EffectThermal radiation: Thermal Radiation

Implementation Method 3

heats the substrate to an oxidation temperature to form an oxide layer on the substrate

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 4

Physical vapor deposition ('PVD') is one common method for coating a substrate

Methodology Applied
Scientific EffectPhysical vapor deposition: Physical Vapour Deposition

Implementation Method 5

A desired evaporation rate of the ceramic material is established during the heating

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS8343591B2Method for use with a coating process
Publication Date: 2013.01.01 RTX CORP
  • US8343591B2 patent drawing
  • US8343591B2 patent drawing

AI summary

A method for use with a coating process includes depositing a ceramic coating on a substrate within a coating chamber. Prior to depositing the ceramic coating, an electron beam source is used to heat a ceramic material. The ceramic material radiates heat to heat a substrate to an oxidation temperature to form an oxide layer on the substrate. A desired evaporation rate of the ceramic material is established during the heating to thereby provide an improved ceramic coating.