Microencapsulated Probiotic Softgel Capsule Manufacturing Process

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Solution Overview

Problem

Probiotic bacteria in softgel capsules face challenges in maintaining viability and stability during storage at room temperature due to high water activity and physical stress during the manufacturing process, leading to rapid decline in colony-forming units (CFU) and ineffective colonization.

Innovation Solution

A process involving microencapsulating probiotic bacteria with a vegetable lipid coating having a melting point between 35°C and 75°C, suspending them in a formulation, mixing at low intensity and temperature, reducing agglomerates, and encapsulating in a softgel capsule to maintain coating integrity and viability, while controlling oxygen exposure.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If probiotic bacteria are placed in softgel capsules for oral delivery, then they can reach the large intestine, but they rapidly lose viability during storage at room temperature due to high water activity and physical stress during manufacturing

Engineering Contradiction:
Improveviability of probiotic bacteriaVSAvoidshelf life at room temperature
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

The probiotic bacteria are pre-coated with a protective lipid coating before encapsulation in the softgel capsule. This preliminary coating action creates a protective barrier that prevents direct contact with the harsh internal environment of the capsule and protects during storage, thereby maintaining viability throughout the shelf life period.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

A lipid coating serves as an intermediary layer between the probiotic bacteria and the softgel capsule environment. This intermediate coating protects the bacteria from physical stress during manufacturing and from the high water activity inside the capsule, enabling both oral delivery and long-term storage at room temperature while maintaining viability.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Stability of the object's composition

If the softgel capsule manufacturing process involves mixing and encapsulation steps, then the probiotic bacteria can be delivered in a stable form, but physical stress during processing compromises cell viability and shelf life

Engineering Contradiction:
Improvestability of probiotic formulationVSAvoidcell viability
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

The lipid coating is applied to the probiotic bacteria before they are subjected to the mixing and encapsulation processes. This preliminary protective action prevents physical stress during processing from directly affecting the bacterial cells, thereby maintaining cell viability while still achieving stable formulation through the subsequent manufacturing steps.

Inventive Principle:
Principle #10Preliminary action

3Duration of action of stationary object

If a protective coating is applied to probiotic bacteria to enhance stability, then shelf life is improved, but the coating must be designed to release probiotics at the appropriate delivery site in the body

Engineering Contradiction:
Improveshelf lifeVSAvoiddesign and application of release mechanism
Core Design Contradiction:
Duration of action of stationary objectVSEase of manufacture

Solution Approach 1:

The lipid coating is designed with specific physical parameters including a melting point between 35°C and 75°C. This parameter change approach allows the coating to remain stable during storage and manufacturing at lower temperatures, while automatically melting and releasing the probiotic bacteria at body temperature in the gastrointestinal tract, thus achieving both long shelf life and appropriate release without complex manufacturing.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process results in a stable softgel capsule with enhanced viability and shelf life of at least 24 months at room temperature, maintaining a high percentage of viable probiotic bacteria for effective colonization.

Implementation Method 1

microencapsulated probiotic bacteria with at least one coating comprising at least one vegetable lipid having a melting point of between 35° C. and 75° C.

Methodology Applied
Scientific EffectPhysical containment: Physical Containment

Implementation Method 2

encapsulating the de-agglomerated fill in a softgel capsule

Methodology Applied
Scientific EffectPhysical containment: Physical Containment

Data Source

PatentUS9427012B2Process of manufacturing a stable softgel capsule containing microencapsulated probiotic bacteria
Publication Date: 2016.08.30 R P SCHERER TECH INC

AI summary

A softgel capsule containing microencapsulated probiotic bacteria is manufactured such that the softgel capsule is stable for at least about 24 months at room temperature.