Process and device for the formation of directly-formed cellulosic webs

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Solution Overview

Problem

Current lyocell melt-blown processes face challenges in washing cellulose filaments, requiring control over filament merging, diameter variation, minimizing damage, controlled liquor exchange, water consumption, and reducing equipment and energy costs, with no prior art achieving all these requirements effectively.

Innovation Solution

A process and device involving a two-stage washing system with a first stage for partial coagulation of cellulose filaments before web formation and a second stage for gentle dewatering, using modular washing modules with controlled wash liquor application and vacuum suction, optimized for line speeds from 5 to 1000 m/min, and incorporating solvent recovery and energy-efficient design.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of substance

If wash liquor is applied to remove solvent from filaments, then solvent removal is improved, but filament damage increases

Engineering Contradiction:
Improvesolvent removalVSAvoidfilament damage
Core Design Contradiction:
Loss of substanceVSObject-affected harmful factors

Solution Approach 1:

The washing process is divided into multiple sequential washing zones (first washing zone, second washing zone, third washing zone) with progressively different wash liquor temperatures and flow rates. This segmentation allows gentle initial washing to remove solvent without damaging filaments, followed by more intensive washing stages, thus resolving the contradiction between effective solvent removal and filament protection

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent employs parameter changes by varying wash liquor temperature across different zones (e.g., cooler temperatures in early zones, warmer temperatures in later zones) and adjusting wash liquor flow rates. These parameter changes enable effective solvent removal while controlling the mechanical stress on filaments, preventing damage during the washing process

Inventive Principle:
Principle #35Parameter changes

2Productivity

If line speed is increased to improve productivity, then production efficiency is improved, but washing quality deteriorates

Engineering Contradiction:
Improveline speedVSAvoidwashing quality
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The washing system is segmented into multiple parallel washing modules within each washing zone, allowing the wash liquor to be distributed across multiple channels. This segmentation maintains adequate washing contact time and quality even at high line speeds, as each module processes a portion of the web simultaneously

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The washing device is designed with multi-functional capabilities that allow it to operate effectively across a wide range of line speeds (5-1000 m/min). The system can adapt its wash liquor application rate, temperature, and flow distribution to maintain washing quality regardless of the production speed, making it universally applicable to different productivity requirements

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Loss of substance

If water consumption is increased to improve solvent removal, then washing effectiveness is improved, but water consumption increases

Engineering Contradiction:
Improvesolvent removalVSAvoidwater consumption
Core Design Contradiction:
Loss of substanceVSQuantity of substance

Solution Approach 1:

The patent employs parameter changes by varying wash liquor temperature across different zones (e.g., cooler temperatures in early zones, warmer temperatures in later zones) and adjusting wash liquor flow rates. These parameter changes enable effective solvent removal while controlling the mechanical stress on filaments, preventing damage during the washing process

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The system is designed to recover and reuse wash liquor from downstream zones in upstream zones, creating a counter-current flow pattern. This recovery approach reduces overall water consumption while maintaining effective solvent removal, as the wash liquor is utilized multiple times across different washing stages

Inventive Principle:
Principle #34Discarding and recovering

4Manufacturing precision

If equipment complexity is increased to control filament merging and diameter variation, then manufacturing precision is improved, but device complexity increases

Engineering Contradiction:
Improvefilament merging controlVSAvoidwashing device complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The washing device is segmented into modular washing modules arranged in sequential zones, where each module performs a specific function (e.g., initial solvent removal, intermediate washing, final rinsing). This modular segmentation achieves precise control over filament properties through staged processing while keeping individual modules relatively simple and manageable

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different sections of the washing device are designed with locally optimized characteristics - for example, the first washing zone uses cooler temperatures and lower flow rates for gentle initial treatment, while later zones use warmer temperatures and higher flow rates for more intensive washing. This local quality differentiation achieves precise filament control without requiring the entire device to be overly complex

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enables efficient production of cellulose-based webs with controlled properties, reduced solvent consumption, and minimized equipment costs, achieving line speeds and product quality not previously possible while maintaining web integrity and environmental sustainability.

Implementation Method 1

Washing of lyocell filaments is a critical process step, in which the solvent has to be removed from the thermoplastic cellulose/solvent threads in a controlled manner

Methodology Applied
Scientific EffectLiquid-liquid extraction: Liquid-Liquid Extraction

Implementation Method 2

a dewatering device (10) for at least partially dewatering the web (11)

Methodology Applied
Scientific EffectSuction: Suction

Data Source

PatentUS11371173B2Process and device for the formation of directly-formed cellulosic webs
Publication Date: 2022.06.28 LENZING AG
  • US11371173B2 patent drawing

AI summary

This invention relates to a process and a device for manufacturing cellulose-based webs which are directly formed from lyocell spinning solution and in particular for the washing of directly formed cellulose webs.