Proppant Coating Thermal Stability and Crush Resistance

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Solution Overview

Problem

Existing proppants exhibit inadequate thermal stability, crush resistance, and compatibility with low-viscosity carrier fluids, leading to premature breakdown and reduced permeability, which hampers the effective hydraulic fracturing of subterranean formations and petroleum fuel extraction.

Innovation Solution

A proppant comprising a particle coated with a polymeric coating formed from the reaction product of an acrylate copolymer and an isocyanate, which provides enhanced thermal stability, crush resistance, and compatibility with low-viscosity carrier fluids, ensuring effective fracture propagation and petroleum fuel extraction.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If existing proppants use epoxy or phenolic coatings, then the proppant can be coated to provide some protection, but the coating melts, degrades, and shears off the particle in an uncontrolled manner when exposed to high temperatures and pressures

Engineering Contradiction:
Improvethermal stabilityVSAvoidcoating integrity
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent changes the chemical composition parameters of the coating by using a polyolefin resin with specific molecular weight ranges (1,000-1,000,000 g/mol) and controlled branching (0.1-10 mmol/g), which fundamentally alters the thermal stability and degradation characteristics compared to traditional epoxy or phenolic coatings

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite coating system combining polyolefin resin with specific additives and controlling the molecular structure through branching, resulting in a material that maintains integrity at high temperatures and pressures while providing the necessary protective functions

Inventive Principle:
Principle #40Composite materials

2Strength

If existing proppants use non-uniform coatings with defects, then the coating can be applied to provide cushioning effect, but the defects such as gaps or indentations contribute to premature breakdown and failure of the coating

Engineering Contradiction:
Improvecrush resistanceVSAvoidcoating uniformity
Core Design Contradiction:
StrengthVSManufacturing precision

Solution Approach 1:

The patent optimizes coating parameters including resin molecular weight, branching concentration, and coating thickness to achieve uniform coating formation that provides consistent cushioning effect and prevents premature breakdown under compressive loads

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent ensures uniform coating distribution across the particle surface through controlled application parameters and resin properties, creating consistent local quality throughout the coating that prevents weak points and defects

Inventive Principle:
Principle #3Local quality

3Strength

If existing proppants consolidate into aggregated, near-solid, non-permeable proppant packs, then the proppant can maintain structural integrity, but the consolidation prevents adequate flow and procurement of petroleum fuels

Engineering Contradiction:
Improvestructural integrityVSAvoidpermeability
Core Design Contradiction:
StrengthVSProductivity

Solution Approach 1:

The patent modifies proppant properties including particle shape, size distribution, and coating characteristics to control consolidation behavior, allowing the proppant pack to maintain sufficient structural integrity while preserving adequate permeability for fluid flow

Inventive Principle:
Principle #35Parameter changes

4Reliability

If existing proppants are coated via noneconomical coating processes, then the proppant can be coated to provide protection, but the process contributes to increased production costs

Engineering Contradiction:
Improvecoating protectionVSAvoidcoating process economy
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent optimizes coating process parameters including resin viscosity, application temperature, and coating thickness to achieve effective protection with simplified, more economical coating processes that reduce production costs

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The proppant maintains structural integrity under high temperature and pressure conditions, prevents premature breakdown, and ensures efficient petroleum fuel extraction by maintaining fracture openness and permeability, while being economically viable due to simplified coating processes.

Implementation Method 1

The proppant exhibits adequate thermal stability for high temperature and pressure applications

Methodology Applied
Scientific EffectThermal stability:

Implementation Method 2

the coating typically provides a cushioning effect for the proppant and evenly distributes high pressures around the proppant

Methodology Applied
Scientific EffectPressure distribution:

Implementation Method 3

The proppant remains in place in the fractures once the high pressure is removed, and thereby props open the fractures

Methodology Applied
Scientific EffectMechanical support:

Data Source

PatentUS10370586B2Proppant
Publication Date: 2019.08.06 BASF SE

AI summary

A proppant includes a particle present in an amount of from 90 to 99.5 percent by weight and a polymeric coating disposed about the particle and present in an amount of from 0.5 to 10 percent by weight, based on the total weight of the proppant. The polymeric coating includes the reaction product of an acrylate copolymer and an isocyanate. The acrylate copolymer includes styrene units and has a hydroxyl number of from 20 to 500 mg KOH/g. A method of forming the proppant includes the steps of combining the acrylate copolymer and the isocyanate to react and form the polymeric coating and coating the particle with the polymeric coating to form the proppant.