3D-Printed Vessel for Proppant Wettability Assessment

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Solution Overview

Problem

Traditional methods for measuring the wettability of fracturing proppants are rudimentary and inaccurate, often relying on visual inspection or indirect methods, which hinders the precise comparison and classification of proppant samples based on their wettability performance.

Innovation Solution

A 3D-printed vessel system for wettability assessment that includes a base component with a threaded cylindrical portion and a cap to level the proppant surface, using a droplet of deionized water or hydrocarbon to measure the contact angle and calculate wettability indices, enabling precise and direct wettability measurements.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If traditional rudimentary methods (naked eye examination or droplet shape judgment) are used for wettability measurement, then the measurement process is simple, but the measurement precision is poor and accurate comparison of proppant samples is hindered

Engineering Contradiction:
Improvewettability measurement precisionVSAvoidmeasurement system complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

A 3D-printed vessel with a standardized flat surface acts as an intermediary between the proppant sample and the droplet. The vessel provides a controlled geometry that ensures consistent droplet placement and contact angle measurement, eliminating the variability of direct measurement on irregular proppant surfaces while maintaining procedural simplicity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention changes the measurement parameter from direct visual inspection of irregular surfaces to contact angle measurement on a standardized flat surface within the vessel. This parameter transformation enables quantitative comparison while keeping the measurement process straightforward

Inventive Principle:
Principle #35Parameter changes

2Measurement precision

If indirect methods (capillary rise method) are used for wettability assessment, then the measurement process is simplified, but the measurement precision deteriorates and accurate classification of proppant samples is not achieved

Engineering Contradiction:
Improvewettability measurement precisionVSAvoidoperation complexity
Core Design Contradiction:
Measurement precisionVSEase of operation

Solution Approach 1:

The invention replaces indirect mechanical methods (capillary rise) with direct optical measurement (contact angle visualization). The flat surface in the vessel allows direct observation and measurement of the droplet contact angle, providing precise wettability data without complex operational procedures

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Measurement precision

If proppant samples with varying wettability performance within the same category are measured using traditional methods, then the measurement process remains consistent, but the ability to accurately compare and distinguish between samples is insufficient

Engineering Contradiction:
Improvesample comparison accuracyVSAvoidproppant sample requirement
Core Design Contradiction:
Measurement precisionVSQuantity of substance

Solution Approach 1:

The invention segments the measurement process into controlled stages: placing a standardized amount of proppant in the vessel, leveling the surface, and then applying the droplet. This segmentation ensures that each measurement is independent and comparable, allowing precise differentiation between samples with similar wettability characteristics

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system provides improved precision and efficiency in wettability assessments, allowing for accurate classification and comparison of proppant samples, reducing measurement time, and minimizing wall effects, thereby enhancing the understanding of proppant wettability characteristics.

Implementation Method 1

The dropping needle of the wettability measurement system applies a droplet of deionized water or a hydrocarbon onto the proppant surface

Methodology Applied
Scientific EffectSurface tension: Surface Tension

Implementation Method 2

wettability assessment of the proppant sample based on the contact angle of the droplet and the proppant sample

Methodology Applied
Scientific EffectWetting: Wetting

Data Source

PatentUS11585742B2Three-dimensional-printed vessel for wettability assessment of fracturing proppants
Publication Date: 2023.02.21 SAUDI ARABIAN OIL CO
  • US11585742B2 patent drawing
  • US11585742B2 patent drawing
  • US11585742B2 patent drawing

AI summary

Systems, methods, and apparatus for a three-dimensional (3D)-printed vessel for wettability assessment of fracturing proppants are disclosed. The vessel includes a base component including a threaded cylindrical portion extending outward from a first side of the base component. The cylindrical portion has a particular thread profile. The base component defines a cavity sized to contain a proppant sample. A cap is configured to be screwed onto the threaded cylindrical portion after the proppant sample is injected into the cavity. A surface of the cap is shaped to flatten a proppant surface of the proppant sample. The cap is threaded with the particular thread profile. A pin is configured to be partially screwed onto a second side of the base component before the proppant sample is injected into the cavity. The second side is opposite to the first side. Other embodiments may be described or claimed.