Propylene Propane Separation Using Absorption Refrigeration

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

The separation of propylene from propane is challenging due to their close boiling points, requiring high-pressure distillation columns and significant reflux, which increases energy consumption and costs, and existing solutions like using a compressor are inefficient.

Innovation Solution

The method employs an absorption refrigerator cooled by chilled water from a waste heat source to reduce condenser pressure, utilizing hot water for heat in the reboiler and optionally low-pressure steam, thereby improving energy efficiency and reducing the need for high-energy compression.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a distillation column operates at high pressure with cooling water at 20-30°C, then the separation of propylene from propane can be achieved, but the condenser pressure becomes high (16 bar a), which limits the feed stream capacity and requires large column diameter

Engineering Contradiction:
Improvefeed stream capacityVSAvoidcondenser pressure
Core Design Contradiction:
ProductivityVSStress or pressure

Solution Approach 1:

The invention changes the temperature parameter of the cooling medium from conventional cooling water at 20-30°C to chilled water at -10 to +10°C. This parameter change allows the condenser to operate at lower pressure (9 bar a instead of 16 bar a) while maintaining the same separation performance, thereby increasing feed stream capacity without requiring larger column diameter

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces the conventional mechanical compression system (compressor requiring electricity or steam turbine) with a thermodynamic absorption refrigeration system that uses waste heat to produce chilled water. This substitution eliminates the need for high-energy compression while achieving the same pressure reduction effect

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Stress or pressure

If a compressor is used to decrease condenser pressure, then the pressure can be reduced, but high value energy such as electricity or high pressure steam is required

Engineering Contradiction:
Improvecondenser pressureVSAvoidenergy consumption
Core Design Contradiction:
Stress or pressureVSUse of energy by moving object

Solution Approach 1:

The invention converts waste heat (a harmful or wasted resource) into a useful resource by using it to drive the absorption refrigeration cycle. The waste heat at 80-90°C provides the thermal energy needed to generate chilled water, thereby achieving pressure reduction without consuming high-value energy like electricity or steam turbine power

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The system uses its own waste heat output to power the refrigeration cycle that produces chilled water for cooling. The process is self-sufficient, using internally generated thermal energy rather than requiring external high-value energy inputs

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach decreases the condenser pressure, allowing for increased feed stream capacity and reducing energy consumption and installation costs by leveraging waste heat for chilling, resulting in a more efficient and economical separation process.

Implementation Method 1

an absorption refrigerator (Y-301) is used to cool chilled water (331)

Methodology Applied
Scientific EffectAbsorption refrigeration: Adsorption Refrigerator

Implementation Method 2

The distillation column C-301 produces 214 t/h of vapor 304 at the top that is condensed against chilled water in a condenser H-302

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

A reboiler H-301 has a duty of 21 MW th and produces 226 t/h of vapor 303

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 4

separation of propylene (propene) from propane... Propylene fractionation separates propylene as a chemical-grade overhead product

Methodology Applied
Scientific EffectDistillation: Distillation

Data Source

PatentEP3509720B1System and method for separation of propylene and propane
Publication Date: 2023.08.09 SABIC GLOBAL TECHNOLOGIES BV
  • EP3509720B1 patent drawingFigure 1
  • EP3509720B1 patent drawingFigure 2
  • EP3509720B1 patent drawingFigure 3

AI summary

A separation system for separating a feed stream comprising propylene and propane and a method for separating such feed stream. The separation system includes a distillation column for producing a light stream comprising propylene and a heavy stream comprising propane; a reboiler for reboiling a part of the first heavy stream to produce a boiled heavy stream; a condenser for cooling the light stream to produce a condensed light stream; and an absorption refrigerator for receiving water and providing chilled water, for receiving hot water from a waste heat source and providing a cooled hot water and for receiving cooling water and providing a heated cooling water. The absorption refrigerator is arranged such that the cooling of the water and the hot water occurs by the cooling water. The condenser is arranged such that the cooling of the light stream occurs by the chilled water from the absorption refrigerator.