Propylene Recovery in FCC Units via Flash Drum Segmentation

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Solution Overview

Problem

In fluid catalytic cracking (FCC) units, propylene and light ends in the unstabilized gasoline used as lean oil for the primary absorber lead to increased load and losses, making high propylene recovery difficult and uneconomical, especially at higher operating pressures.

Innovation Solution

A process involving a primary absorber feed flash drum to decrease propylene and light ends in unstabilized gasoline, where a portion of the liquid fraction is heated and sent to a flash drum to produce a flashed light ends stream, which is then sent to the wet gas compressor train, and the bottoms liquid stream is further heated and routed to the FCC gas concentration absorber, optimizing propylene and LPG recovery.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of substance

If conventional overhead condensing and receiving steps are used, then propylene can be recovered from FCC fractionator overhead, but the liquid phase carries considerable propylene and light ends to the primary absorber, increasing load and losses

Engineering Contradiction:
Improvepropylene lossVSAvoidequipment design complexity
Core Design Contradiction:
Loss of substanceVSDevice complexity

Solution Approach 1:

The invention divides the liquid phase handling into two separate streams: a first portion sent to the primary absorber and a second portion routed to a flash drum for light ends removal. This segmentation allows propylene-rich liquid to be separated from light ends before absorber feed, reducing propylene loss while maintaining simple equipment design

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention extracts light ends and excess propylene from the liquid phase by routing a portion of the liquid to a flash drum operated at reduced pressure. The flashed vapor containing light ends and propylene is removed and sent to fuel gas, preventing these components from loading the primary absorber

Inventive Principle:
Principle #2Taking out (Extraction)

2Loss of substance

If unit operating pressures at main column receiver are increased, then propylene recovery becomes more difficult, but higher pressures favor more propylene in the liquid phase

Engineering Contradiction:
Improvepropylene lossVSAvoidoperating pressure
Core Design Contradiction:
Loss of substanceVSStress or pressure

Solution Approach 1:

The invention changes the pressure parameter by operating the flash drum at reduced pressure (e.g., 0.5-2.0 atm) compared to the main column receiver. This pressure reduction causes light ends and propylene to flash into vapor phase, separating them from the liquid phase sent to the primary absorber, thereby reducing propylene loss regardless of main column operating pressure

Inventive Principle:
Principle #35Parameter changes

3Loss of substance

If propylene in unstabilized gasoline is reduced, then propylene recovery improves, but additional equipment modifications are required

Engineering Contradiction:
Improvepropylene lossVSAvoidequipment modification requirement
Core Design Contradiction:
Loss of substanceVSEase of manufacture

Solution Approach 1:

The invention makes the flash drum a multi-functional unit that handles both light ends removal and propylene enrichment. The flash drum serves to separate light ends from propylene-rich liquid while also providing a pressure reduction stage, eliminating the need for multiple separate equipment modifications

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The flash drum uses its own vapor-liquid equilibrium characteristics at reduced pressure to automatically separate light ends and propylene from the liquid phase. The process is self-regulating based on pressure and temperature conditions, requiring minimal additional control equipment

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This process enhances propylene and LPG recovery by reducing losses, making the process more economical and feasible for existing FCC units without requiring significant equipment modifications, achieving near 99.6% propylene recovery and reducing the load on the wet gas compressor.

Implementation Method 1

feeding the heated stream to a flash drum to produce a flashed light ends stream and a bottoms liquid stream

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

feeding a second portion of the liquid fraction obtained in step (iii) to at least one heat exchanger to produce a heated stream

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 3

routing the liquid stream to a FCC gas concentration absorber

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Data Source

PatentEP3390329B1Process for improving propylene recovery from FCC recovery unit
Publication Date: 2023.09.20 UOP LLC
  • EP3390329B1 patent drawingFigure 1
  • EP3390329B1 patent drawingFigure 2
  • EP3390329B1 patent drawingFigure 3

AI summary

The present subject matter relates generally to processes for propylene recovery. More specifically, the present subject matter relates to processes for enhanced recovery of propylene and liquid petroleum gas (LPG) from the fuel gas produced in fluid catalytic cracking (FCC) units by minimizing the light ends and propylene in the unstabilized gasoline which is used as lean oil for the primary absorber of the FCC gas concentration unit.