Purified Protease Complex for Animal Feed via Isoelectric Focusing

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Solution Overview

Problem

Existing enzymatic complexes from Streptomyces fradiae for animal nutrition and therapeutic applications are not completely free of biological impurities, which can affect their activity and efficacy, and lack precise characterization and separation of proteases based on their isoelectric points.

Innovation Solution

A purified enzymatic complex is developed, comprising proteases with isoelectric points of approximately 7.0 and 8.0, obtained through fermentation, ultrafiltration, ion exchange chromatography, and isoelectrofocusing, with a specific activity of 150,000 and 38,000 Anson units/mg of proteins respectively, and a process that ensures the removal of filler substances devoid of proteolytic activity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If existing enzymatic complexes from Streptomyces fradiae are used for animal nutrition, then proteolytic activity is provided, but biological impurities remain that affect activity and efficacy

Engineering Contradiction:
ImproveefficacyVSAvoidbiological impurities
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The complex proteolytic activity is segmented into distinct proteases with different isoelectric points (pI around 7.0 and pI around 8.0). This segmentation allows selective purification of individual protease types through isoelectric focusing, separating them from biological impurities while maintaining their beneficial proteolytic functions in animal nutrition

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent extracts and isolates specific proteases from the Streptomyces fradiae fermentation broth using a multi-step purification process including ultrafiltration, ion exchange chromatography, and isoelectric focusing. This extraction removes biological impurities while concentrating the active proteolytic enzymes for reliable use in animal feed

Inventive Principle:
Principle #2Taking out (Extraction)

2Measurement precision

If proteases are not separated and characterized by isoelectric point, then production is simpler, but precise characterization and control of enzyme activity is lost

Engineering Contradiction:
Improveenzyme characterizationVSAvoidpurification process
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent utilizes the isoelectric point (pI) parameter as a key characteristic to differentiate and purify specific proteases from Streptomyces fradiae. By controlling pH during isoelectric focusing, the method achieves precise separation and characterization of proteases with pI around 7.0 and pI around 8.0, enabling accurate measurement and control of enzyme activity despite the added purification steps

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The complex provides precise therapeutic effects, improves animal health and growth, reduces food consumption, and increases profitability in industrial farming by ensuring a technically defined and active product with enhanced proteolytic activity and reduced contamination.

Implementation Method 1

The strain of Streptomyces fradiae can produce at least five types of proteases designated Ia, Ib, II, III, IV and two peptidases

Methodology Applied
Scientific EffectProteolysis: Hydrolysis

Implementation Method 2

extraction of the complex by filtration, then ultrafiltration on a membrane having a cut-off threshold corresponding to a molecular weight of between 2000 and 12,000

Methodology Applied
Scientific EffectUltrafiltration: Semipermeable Membrane

Implementation Method 3

ion exchange chromatography followed by isoelectrofocusing

Methodology Applied
Scientific EffectIon exchange: Ion Exchange

Implementation Method 4

among these proteases in the mixture one of them has an isoelectric point of around 7.0 and a specific activity of approximately 150,000 units Anson / mg of proteins and another protease has an isoelectric point of the order of 8.0

Methodology Applied
Scientific EffectIsoelectric focusing: Isoelectric Focusing

Implementation Method 5

finally the complex obtained is lyophilized

Methodology Applied
Scientific EffectLyophilization: Freeze Drying

Data Source

PatentEP2735235B1Use of an enzyme complex in the feed of farm animals
Publication Date: 2019.04.24 HOOREMAN HERVE
  • EP2735235B1 patent drawingFigure 1~2
  • EP2735235B1 patent drawingFigure 3~4

AI summary

Supplementing farm animal feed, involves adding an enzymatic complex comprising a mixture of proteases obtained by culturing a Streptomyces fradiae strain to farm animal feed, where among this mixture of proteases one of them has an isoelectric point of 7 and another has an isoelectric point of 8. Independent claims are included for 1) feed composition for farm animals comprising: the enzymatic complex comprising a mixture of proteases obtained by culturing a Streptomyces fradiae strain, and optionally including excipients or vehicles for nutriments; and 2) manufacturing the enzymatic complex involving: culturing the Streptomyces fradiae strain, filtering the fermentation broth, then extracting the enzymatic complex by ultrafiltration and ion exchange chromatography followed by an isoelectric focusing, and finally, lyophilizing the complex thus obtained.