Pt-Pd Diesel Catalyst Zeolite Light-Off

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Solution Overview

Problem

Diesel engines face challenges in reducing emissions of particulate matter, nitrogen oxides, unburned hydrocarbons, and carbon monoxide due to high light-off temperatures and potential poisoning effects of palladium in oxidation catalysts, which hinder effective conversion of pollutants, especially during cold-start periods.

Innovation Solution

A catalytic article comprising a Pt/Pd diesel oxidation catalyst with a zeolite that minimizes negative interactions between platinum group metals and the zeolite, using a high-surface area refractory metal oxide support with a silica-to-alumina molar ratio greater than 1200, and specific zeolite frameworks like beta, MFI, and MWW to enhance CO/HC light-off and storage functions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a Pt/Pd diesel oxidation catalyst is used to treat exhaust emissions, then the oxidation of hydrocarbons and carbon monoxide is enhanced, but the high light-off temperature and palladium poisoning effects hinder effective conversion during cold-start periods

Engineering Contradiction:
Improveoxidation efficiencyVSAvoidlight-off temperature
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The patent changes the chemical composition parameters of the catalyst by incorporating specific zeolite structures (beta, MFI, or MWW) with controlled silica-to-alumina ratios (15-100), and optimizing the Pt:Pd ratio (1:4 to 4:1). These parameter changes enable the catalyst to achieve effective oxidation at lower temperatures while maintaining high conversion efficiency during cold-start periods

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite catalyst material combining platinum group metals (Pt and Pd) with zeolite structures supported on high-surface-area refractory metal oxide. This composite structure synergistically combines the oxidation activity of Pt/Pd with the hydrocarbon storage and low-temperature promotion capabilities of zeolite, resolving the contradiction between oxidation efficiency and light-off temperature

Inventive Principle:
Principle #40Composite materials

2Productivity

If palladium is used in the oxidation catalyst to reduce cost and maintain activity, then catalytic conversion is improved, but palladium poisoning effects occur that reduce catalyst performance

Engineering Contradiction:
Improvecatalytic conversionVSAvoidcatalyst stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent optimizes the Pd content and Pt:Pd ratio within specific ranges (Pt:Pd from 1:4 to 4:1) to balance cost and performance. This parameter optimization prevents excessive Pd accumulation that causes poisoning while maintaining sufficient catalytic activity for effective exhaust treatment

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The zeolite component acts as an intermediary that protects the Pt/Pd active sites from poisoning effects. The zeolite structure adsorbs harmful substances and regulates the interaction between Pd and the support material, thereby maintaining catalyst stability and preventing deactivation

Inventive Principle:
Principle #24Intermediary (Mediator)

3Quantity of substance

If zeolite is used to store hydrocarbons during cold-start periods, then HC storage function is improved, but premature release of stored hydrocarbons occurs that reduces treatment efficiency

Engineering Contradiction:
Improvehydrocarbon storage capacityVSAvoidhydrocarbon retention time
Core Design Contradiction:
Quantity of substanceVSLoss of time

Solution Approach 1:

The patent carefully controls the silica-to-alumina ratio of the zeolite (15-100) and selects specific zeolite structures (beta, MFI, or MWW) to optimize the balance between HC storage capacity and release timing. These parameter adjustments ensure that hydrocarbons are stored during cold-start and released at the appropriate time for complete oxidation, preventing premature release

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution effectively oxidizes hydrocarbons and carbon monoxide to carbon dioxide and water, reduces light-off temperatures, and prevents premature release of stored hydrocarbons, thereby improving diesel engine exhaust treatment efficiency and reducing emissions.

Implementation Method 1

a zeolite and a platinum group metal (PGM) comprising platinum and palladium supported on a high surface area refractory metal oxide support such that the zeolite minimizes negative interactions of these platinum group metals with the zeolite

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

a catalytic article comprising a Pt/Pd diesel oxidation catalyst with carbon monoxide/hydrocarbon (CO/HC) light-off and hydrocarbon (HC) storage functions

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

The solution effectively oxidizes hydrocarbons and carbon monoxide to carbon dioxide and water

Methodology Applied
Scientific EffectOxidation: Oxidation

Data Source

PatentEP2834002B1Pt-pd diesel oxidation catalyst with co/HC light-off and HC storage function
Publication Date: 2019.03.20 BASF CORPORATON
  • EP2834002B1 patent drawingFigure 1~2
  • EP2834002B1 patent drawingFigure 3

AI summary

A diesel oxidation catalyst for the treatment of exhaust gas emissions, such as the oxidation of unburned hydrocarbons (HC), and carbon monoxide (CO) and the reduction of nitrogen oxides (NOx) is described. More particularly, the present invention is directed to a washcoat composition comprising high silica to alumina zeolite and platinum and palladium such that the zeolite minimizes negative interactions of these platinum group metals with the zeolite.