PVD Coating Flow Control via Knudsen Number Regulation

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Solution Overview

Problem

In PVD coating processes, the reduction of pressure in the coating chamber leads to uncontrolled movement of vapor particles, resulting in undesirable scattered coatings due to the increased mean free path length, making it difficult to transport the coating material to the workpiece in a targeted manner.

Innovation Solution

The method involves regulating the pressure and temperature in the coating chamber to achieve a Knudsen number (Kn) of ≤0.1, ensuring a continuum or gliding flow, allowing for controlled deposition of the coating material on the workpiece by adjusting the pressure, temperature, and distance between the inflow point and the workpiece, thereby reducing stray coatings.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If the pressure in the coating chamber is reduced to enable PVD coating, then the vapor particles can reach the workpiece, but the mean free path length increases causing uncontrolled movement and scattered coatings

Engineering Contradiction:
Improvetargeted deposition of coating materialVSAvoidpressure and temperature regulation system
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The invention changes the physical parameters of the coating material by controlling temperature and pressure to achieve a specific Knudsen number range (0.01 ≤ Kn ≤ 0.1). This parameter control transforms the vapor transport from uncontrolled molecular flow to controlled continuum or gliding flow, enabling targeted deposition while maintaining reduced pressure conditions necessary for PVD coating.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention dynamically adjusts the flow regime by regulating temperature and pressure parameters during the coating process. By maintaining the Knudsen number within the specified range, the system transitions between different flow regimes (continuum, gliding, or transition flow) to optimize the transport of coating material to the workpiece, making the process adaptable and controllable.

Inventive Principle:
Principle #15Dynamics

2Productivity

If the pressure is reduced in the coating chamber, then vapor particles can travel to the workpiece, but stochastic movements dominate making flow transport difficult

Engineering Contradiction:
Improvecoating material transport efficiencyVSAvoidcontrolled deposition
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The invention optimizes the Knudsen number to a specific range (0.01 ≤ Kn ≤ 0.1) by adjusting temperature and pressure parameters. This ensures the coating material transport operates in the continuum or gliding flow regime, where viscous forces dominate over molecular randomness, enabling both efficient transport and controlled deposition on the workpiece.

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If heating surfaces of the coating chamber is used to reduce stray coatings, then scattered coatings are reduced, but the process becomes complex and energy-intensive

Engineering Contradiction:
Improvereduction of stray coatingsVSAvoidenergy consumption for heating
Core Design Contradiction:
Manufacturing precisionVSUse of energy by stationary object

Solution Approach 1:

The invention applies preliminary action by controlling the Knudsen number and establishing continuum or gliding flow conditions before deposition occurs. This preventive approach ensures coating material is transported in a controlled manner from the source to the workpiece, preventing stray coatings from forming in the first place, rather than requiring subsequent heating measures to mitigate scattered coatings.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention converts the typically harmful effect of reduced pressure (which causes uncontrolled vapor movement) into a beneficial condition by operating at an optimized Knudsen number range. The reduced pressure is maintained for efficient PVD coating, but the specific parameter control transforms the vapor transport into a controlled flow regime that prevents stray coatings without requiring additional heating energy.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables a controllable flow of the coating material, significantly reducing stray coatings and ensuring targeted deposition on the workpiece, making the process more efficient and effective.

Implementation Method 1

a coating material, which is initially in solid or liquid form, is usually vaporized by physical processes. This can be done, for example, thermally by directly heating the coating material

Methodology Applied
Scientific EffectThermal vaporization: Evaporation

Implementation Method 2

by bombarding it with an electron or ion beam

Methodology Applied
Scientific EffectElectron beam vaporization: Electron Beam

Implementation Method 3

or by illuminating it with a laser beam

Methodology Applied
Scientific EffectLaser vaporization: Laser Ablation

Implementation Method 4

PVD stands for physical vapor deposition... the vapor particles of the vaporized coating material can reach the workpiece to be coated

Methodology Applied
Scientific EffectPhysical vapor deposition: Physical Vapour Deposition

Implementation Method 5

the vapor particles condense on all surfaces of the coating chamber whose temperature is below the condensation temperature

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 6

At Kn ≤ 0.01 one speaks of a continuum flow... According to the invention, the process parameters of pressure and temperature are selected in such a way that there is a continuum flow or at least a gliding flow during the coating process

Methodology Applied
Scientific EffectContinuum flow:

Implementation Method 7

Knudsen numbers between 0.01 and 0.1 indicate that the flow under consideration is a gliding flow

Methodology Applied
Scientific EffectGliding flow:

Data Source

PatentEP3660181A1Method for pvd coating of workpieces
Publication Date: 2020.06.03 THYSSENKRUPP STEEL EUROPE AG PATENTE PATENT DEPARTMENT
  • EP3660181A1 patent drawingFigure 1~2
  • EP3660181A1 patent drawing
  • EP3660181A1 patent drawing

AI summary

A method for PVD coating of a workpiece (1) with a coating material (2) is proposed, wherein the workpiece (1) is provided in a coating chamber, the pressure in the coating chamber is regulated, the coating material (2) flows into the coating chamber at an inlet point (3), the coating material (2) is tempered to a temperature, and the pressure and temperature of the coating material (2) are set such that the equation Kn=kBT2πσ2pl with Kn ≤ 0.1 is satisfied, where T is the temperature of the coating material (2), kB is the Boltzmann constant, σ is the diameter of the molecules of the coating material (2), p is the pressure, and I is the characteristic length, typically the distance between the inlet point (3) and the workpiece (1).