Water-Soluble Unit Dose Film Composition for Cold-Wash Dissolution

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Solution Overview

Problem

Water-soluble unit dose articles made with traditional polyvinyl alcohol films face issues of incomplete dissolution during short and cold wash cycles, leading to undissolved film material deposition, and seal failures between the films result in premature rupture.

Innovation Solution

A water-soluble unit dose article comprising a first and second water-soluble film, where the first film contains a blend of polyvinyl alcohol polymers with carboxylated anionic monomer units and a higher proportion of homopolymer, and the second film consists mainly of polyvinyl alcohol homopolymer with a specific viscosity, sealed using a solvent sealing solution predominantly composed of water, to enhance film integrity and reduce seal failures.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If traditional polyvinyl alcohol films are used in water-soluble unit dose articles, then the films provide sufficient structural integrity during storage and transport, but the films suffer from incomplete dissolution during short and cold wash cycles resulting in undissolved film material deposition

Engineering Contradiction:
Improvestructural integrityVSAvoiddissolution completeness
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The patent modifies the chemical composition parameters of the polyvinyl alcohol film by incorporating carboxylated anionic monomer units (3-6 mol.%) and adjusting the blend ratio between copolymer and homopolymer. These parameter changes enable the film to maintain structural integrity while achieving complete dissolution under short and cold wash conditions, resolving the contradiction between reliability and productivity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite polyvinyl alcohol material by blending two different PVOH polymers with distinct properties: one providing structural strength and the other enhancing dissolution. This composite approach allows the film to exhibit both sufficient structural integrity and complete dissolution behavior, simultaneously addressing both requirements.

Inventive Principle:
Principle #40Composite materials

2Productivity

If polyvinyl alcohol films with higher homopolymer content are used to improve dissolution, then dissolution performance improves, but seal failures occur resulting in premature rupture

Engineering Contradiction:
Improvedissolution completenessVSAvoidseal integrity
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent optimizes the compositional parameters by limiting homopolymer content to 35-90% (rather than using high homopolymer content) and adjusting the carboxylated monomer unit content to 3-6 mol.%. This balanced parameter selection ensures both complete dissolution and adequate seal integrity, preventing the premature rupture caused by excessive homopolymer content.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies different polymer compositions to different functional regions: the film body uses a balanced blend for dissolution, while the seal areas maintain sufficient polymer strength for sealing reliability. This local differentiation of material properties allows the film to achieve complete dissolution without compromising seal integrity.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution ensures complete dissolution of the film under short and cold wash cycles while maintaining structural integrity and reducing seal failures, ensuring the contents are released into the wash liquor effectively.

Implementation Method 1

sealed using a solvent sealing solution predominantly composed of water

Methodology Applied
Scientific EffectSolvent sealing: Solvation

Implementation Method 2

when the water-soluble unit dose article is added to water, the film dissolves/disintegrates releasing the internal contents into the surrounding water

Methodology Applied
Scientific EffectDissolution: Solvation

Data Source

PatentEP4015569B1Water-soluble unit dose article
Publication Date: 2026.04.01 PROCTER & GAMBLE CO
  • EP4015569B1 patent drawingFigure 1
  • EP4015569B1 patent drawingFigure 2

AI summary

Water-soluble unit dose article and a method of making.