Low-Dusting Granular PVPP via Roller Compaction

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Solution Overview

Problem

Current crosslinked polyvinylpyrrolidone (PVPP) products experience dusting issues during material handling, leading to material loss and handling problems, especially in the beverage industry, where particle size affects performance, and existing solutions do not address dusting without compromising binding capacity.

Innovation Solution

The production of low-dusting PVPP compositions involves compressing a PVPP feedstock and breaking it into granules or grains, with less than 10% of particles being 100 μm or smaller, and incorporating co-ingredients like cellulose or bentonite clay to enhance handling and performance, using methods like roller compaction and granulation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If PVPP is processed to reduce particle size for improved performance, then polyphenol absorptive capacity is improved, but dusting increases during material handling

Engineering Contradiction:
Improvepolyphenol absorptive capacityVSAvoiddusting
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The PVPP is compressed into a compacted mass and then broken into granules with controlled size distribution, segmenting the material to reduce dust while maintaining performance

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The particle size distribution is modified through compression and breaking processes to achieve granules where particles 100 μm or smaller comprise less than 10% by weight, changing the physical parameter to reduce dusting

Inventive Principle:
Principle #35Parameter changes

2Reliability

If PVPP particle size is reduced to enhance binding capacity, then polyphenol removal efficiency is improved, but material loss increases

Engineering Contradiction:
Improvepolyphenol removal efficiencyVSAvoidmaterial loss
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The PVPP is pre-compressed into a compacted form before breaking, which preliminary consolidates the material to prevent excessive dusting and material loss during subsequent handling

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The particle size distribution is controlled through the compression and breaking process to optimize the balance between surface area for binding and particle size for reduced material loss

Inventive Principle:
Principle #35Parameter changes

3Reliability

If PVPP is used in fine particle form for optimal performance, then beverage clarification is improved, but handling difficulty increases

Engineering Contradiction:
Improvebeverage clarificationVSAvoidmaterial handling
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The PVPP is segmented into granules with controlled size distribution through compression and breaking, making the material easier to handle while maintaining clarification performance

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The compressed and broken PVPP forms a composite granular structure that combines the clarifying effectiveness of fine particles with the handling ease of larger granules

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The granulated PVPP products are substantially dust-free while maintaining polyphenol absorptive capacity, offering improved material handling and performance without special equipment, with co-ingredients enhancing functionality and retaining 80% or more of the original polyphenol removal efficiency.

Implementation Method 1

The complexations through hydrogen bonding and/or dipolar interactions also enable PVPP to serve as a dye scavenger

Methodology Applied
Scientific EffectHydrogen bonding: Chemical Bonding

Implementation Method 2

The complexations through hydrogen bonding and/or dipolar interactions also enable PVPP to serve as a dye scavenger

Methodology Applied
Scientific EffectDipolar interactions: Chemical Bonding

Implementation Method 3

compressing a PVPP feedstock and breaking it into granules or grains

Methodology Applied
Scientific EffectMechanical force: Mechanical Force

Implementation Method 4

using methods like roller compaction and granulation

Methodology Applied
Scientific EffectCompression: Compression

Data Source

PatentUS10988611B2Crosslinked polyvinylpyrrolidone compositions
Publication Date: 2021.04.27 LLC ASHLAND
  • US10988611B2 patent drawing
  • US10988611B2 patent drawing
  • US10988611B2 patent drawing

AI summary

Low-dusting, granular compositions are provided that comprise at least 15% by weight crosslinked polyvinylpyrrolidone.