Pyrethroid Granules via Silica Adsorption and Block Copolymer

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Solution Overview

Problem

Existing pesticide formulations, particularly those containing pyrethroid insecticides, face challenges with dustiness, flowability, and storage stability, and often require solvents that can be hazardous and volatile, limiting their concentration and application efficiency.

Innovation Solution

A non-dusty, free-flowing, storage-stable solid composition is achieved by combining silica and kaolin with a block copolymer of ethylene oxide and propylene oxide in specific ratios, eliminating the need for solvents and enabling high concentrations of liquid active ingredients in granular form, which enhances dispersibility and suspensibility.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If organic solvents are used in liquid formulations to achieve desired solubility and concentration of active ingredients, then the formulation can be diluted and applied effectively, but the formulation becomes flammable, toxic, and causes irritation to the human body

Engineering Contradiction:
Improveconcentration of active ingredientVSAvoidtoxicity and flammability
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The invention extracts and eliminates the harmful organic solvent component from the formulation while retaining the active ingredient through alternative means (co-crystallization with inert solid carriers), thereby removing toxicity and flammability hazards

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention changes the physical state parameter of the active ingredient from liquid (requiring organic solvents) to solid (co-crystallized form), which eliminates the need for flammable solvents while maintaining deliverability

Inventive Principle:
Principle #35Parameter changes

2Ease of operation

If dry powdery composition is used to achieve easy application, then the formulation can be easily handled and diluted, but it causes dust formation, nozzle choking, sedimentation, and lumping during storage

Engineering Contradiction:
Improveease of handling and dilutionVSAvoiddust formation and nozzle choking
Core Design Contradiction:
Ease of operationVSObject-generated harmful factors

Solution Approach 1:

The invention segments the active ingredient into micro-crystalline particles distributed within a solid matrix of inert carriers, creating a granular structure that prevents dust formation while maintaining ease of handling

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention creates a composite material system combining the active ingredient with inert solid carriers (silica, kaolin, attapulgite) in a co-crystallized granular structure, which eliminates dustiness while preserving ease of operation

Inventive Principle:
Principle #40Composite materials

3Reliability

If liquid formulations with high concentration of pyrethroids are used to achieve effective pest control, then the formulation displays strong insecticidal activity, but it suffers from high volatility and flammability

Engineering Contradiction:
Improveinsecticidal activityVSAvoidvolatility and flammability
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The invention changes the physical state of the liquid pyrethroid active ingredient into a solid co-crystallized form, which dramatically reduces volatility and eliminates flammability while preserving insecticidal activity

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention converts the harmful volatility and flammability characteristics of liquid pyrethroids into benefits by transforming them into a stable solid co-crystallized formulation that maintains effectiveness while eliminating safety hazards

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

4Shape

If granules are produced by conventional methods to achieve solid composition form, then the formulation can be applied to water surface or soil, but it requires organic solvents that are flammable and toxic

Engineering Contradiction:
Improvegranular formVSAvoidtoxicity and flammability
Core Design Contradiction:
ShapeVSObject-affected harmful factors

Solution Approach 1:

The invention extracts and removes the harmful organic solvent step from the granulation process, achieving granular formulation through direct co-crystallization of the active ingredient with inert solid carriers

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention enables the active ingredient to self-organize into a stable granular co-crystallized structure with inert carriers without requiring external organic solvents, achieving both granular form and safety simultaneously

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides a stable, environmentally friendly, and cost-effective formulation with improved dispersibility and suspensibility, allowing for higher concentrations of pyrethroid insecticides without the risks associated with solvent use, ensuring effective application and reduced environmental impact.

Implementation Method 1

a non dusty, free flowing, storage stable solid composition comprising of at least one pesticide from pyrethroid class... brought about by a combination of inert ingredients silica and kaolin

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

block copolymer of ethylene oxide and propylene oxide in specific proportions... improved properties of dispersibility and suspensibility

Methodology Applied
Scientific EffectSurfactant action: Surfactant

Data Source

PatentUS9220271B2Non-dusty, free flowing, storage stable solid composition and a process for its preparation
Publication Date: 2015.12.29 UNITED PHOSPHORUS INC

AI summary

A solid water dispersible granular composition of pesticide comprising up to 50% of at least one pesticide from pyrethroid class, more particularly a highly viscous liquid pyrethroid insecticide, permethrin, having the properties of excellent dispersibility and suspensibility, as well as the process of preparation of the composition are disclosed. Also the improved storage stability, dispersibility and suspensibility properties are discussed for this granular composition.