Pyrimidine-Based Electrolyte for Lithium Battery SEI Stability

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Solution Overview

Problem

Conventional lithium secondary batteries face issues with the stability of the solid electrolyte interface (SEI) layer at high temperatures, leading to increased inner pressure and poor conductivity at low temperatures, which affects their performance and life cycle.

Innovation Solution

A non-aqueous electrolyte solution comprising a pyrimidine-based compound, a non-fluorinated solvent, and a fluorinated solvent, with a fluorine content range of 0.1 to 50 wt%, is used to form a stable and durable SEI layer, enhancing the battery's high-temperature stability and life characteristics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If a large amount of ethylene carbonate is used in the electrolyte solution, then the battery can maintain stable structure, but the SEI layer stability at high temperature deteriorates and inner pressure increases

Engineering Contradiction:
Improvebattery structure stabilityVSAvoidSEI layer stability at high temperature
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

The patent changes the chemical composition parameters of the electrolyte by introducing fluorinated cyclic carbonate compounds with specific fluorine content (0.1-50 wt%) and pyrimidine-based compounds (0.01-5 wt%). This parameter change modifies the SEI layer formation characteristics, enabling stable SEI layers at high temperatures while maintaining battery structure stability.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite electrolyte system by combining fluorinated cyclic carbonate (which forms stable SEI), non-fluorinated cyclic carbonate (which provides ionic conductivity), and pyrimidine-based compounds (which enhance SEI stability). This composite approach synergistically resolves the contradiction between structure stability and SEI layer stability.

Inventive Principle:
Principle #40Composite materials

2Stability of the object's composition

If ethylene carbonate is used to maintain battery structure, then structural stability is improved, but conductivity at low temperature deteriorates

Engineering Contradiction:
Improvebattery structure stabilityVSAvoidionic conductivity at low temperature
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

The patent modifies the electrolyte composition by incorporating fluorinated cyclic carbonate compounds that have lower freezing points and better low-temperature fluidity compared to conventional ethylene carbonate. This parameter change maintains structural stability while improving low-temperature ionic conductivity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies different functional components to different temperature conditions: fluorinated cyclic carbonate provides low-temperature conductivity, while pyrimidine-based compounds ensure high-temperature SEI stability. This local quality approach addresses temperature-dependent performance variations.

Inventive Principle:
Principle #3Local quality

3Ease of manufacture

If conventional electrolyte composition is used, then manufacturing simplicity is maintained, but battery life cycle at high temperature deteriorates

Engineering Contradiction:
Improveelectrolyte preparation simplicityVSAvoidbattery life cycle at high temperature
Core Design Contradiction:
Ease of manufactureVSDuration of action of stationary object

Solution Approach 1:

The patent modifies the electrolyte composition parameters by adding specific fluorinated cyclic carbonate and pyrimidine-based compounds in defined concentrations. These parameter changes enhance high-temperature life cycle while maintaining compatibility with existing manufacturing processes.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The pyrimidine-based compound acts as an intermediary substance that mediates between the fluorinated cyclic carbonate and the anode surface, forming a stable SEI layer that protects against high-temperature degradation. This intermediary mechanism extends battery life without complicating manufacturing.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution significantly improves the life cycle and stability of lithium secondary batteries at both room and high temperatures, minimizing capacity decrease and maintaining high-rate charging/discharging performance.

Implementation Method 1

lithium ions emitted from a cathode active material such as a lithium-metal oxide is transferred into an anode active material such as graphite and inserted between the layers of the anode active material, at which high reactive lithium reacts with the electrolyte solution and carbon present in the anode active material on the surface of the anode active material such as graphite to produce a compound such as Li 2 CO 3 , Li 2 O and LiOH

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 2

The SEI layer functions as an ion tunnel, allowing only lithium ions to pass through. As an effect of such an ion tunnel, the SEI layer prevents the molecule of an organic solvent having large molecular weight, which is included in the electrolyte solution and transferred together with lithium ions, from being inserted between the layers of the anode active material

Methodology Applied
Scientific EffectIon transport: Ion Exchange

Implementation Method 3

The non-aqueous electrolyte solution according to one aspect of the present invention, which comprises a fluorinated solvent, a non-fluorinated solvent and a pyrimidine-based compound, is used in a lithium secondary battery to minimize the capacity decrease and provide a markedly improved life characteristics and stability even if charging/discharging cycles are repeated several hundred times at room temperature and at high temperature

Methodology Applied
Scientific EffectThermal stability enhancement:

Data Source

PatentEP2736112B1Nonaqueous electrolyte and lithium secondary battery using same
Publication Date: 2018.02.21 LG CHEM LTD
  • EP2736112B1 patent drawingFigure 1~2
  • EP2736112B1 patent drawingFigure 3
  • EP2736112B1 patent drawing

AI summary

The present invention provides non-aqueous electrolyte solution for a lithium secondary battery, comprising a pyrimidine-based compound, a non-fluorinated solvent and a fluorinated solvent; and a lithium secondary battery using the same.