Pyrimidine Derivative Electron Transport Layer for OLED Voltage Reduction

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Solution Overview

Problem

Multilayer organic light emitting display devices with charge generation layers experience increased operating voltage and decreased efficiency, particularly when N-type charge generation layers are doped with alkali metals, leading to reduced lifetime and electron injection issues due to energy level differences.

Innovation Solution

Incorporating a pyrimidine derivative as an electron transport layer with high electronegativity in at least one of the light emitting parts, which facilitates charge transport and reduces operating voltage while improving efficiency by enhancing electron mobility and injection properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Duration of action of stationary object

If a multilayer emitting structure with charge generation layers is used, then device lifetime is improved, but operating voltage increases and efficiency decreases

Engineering Contradiction:
Improvedevice lifetimeVSAvoidoperating voltage
Core Design Contradiction:
Duration of action of stationary objectVSUse of energy by stationary object

Solution Approach 1:

The patent modifies the energy level parameters of the charge generation layers by selecting materials with specific HOMO and LUMO levels. The P-type CGL uses materials with HOMO levels of 5.8-6.5 eV, while the N-type CGL uses materials with LUMO levels of 2.0-3.0 eV, creating optimized energy level梯度的 that reduces voltage requirements while maintaining device lifetime

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs composite material structures where the charge generation layers are composed of multiple organic compounds with complementary properties. The P-type CGL combines materials like TCTA and TAPC, while the N-type CGL combines materials like BCP and TPBi, creating synergistic effects that simultaneously improve lifetime and reduce operating voltage

Inventive Principle:
Principle #40Composite materials

2Duration of action of stationary object

If a multilayer emitting structure with charge generation layers is used, then device lifetime is improved, but emission efficiency decreases

Engineering Contradiction:
Improvedevice lifetimeVSAvoidemission efficiency
Core Design Contradiction:
Duration of action of stationary objectVSProductivity

Solution Approach 1:

The patent optimizes the thickness parameters of the charge generation layers to balance lifetime and efficiency. The P-type CGL is designed with thickness of 5-20 nm and the N-type CGL with thickness of 5-15 nm, creating optimal charge distribution that enhances emission efficiency while maintaining long device lifetime through the multilayer structure

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies different material compositions and thicknesses to different regions of the charge generation layers. The P-type CGL uses materials with higher hole mobility near the anode interface, while the N-type CGL uses materials with higher electron mobility near the cathode interface, creating locally optimized charge transport that improves overall emission efficiency

Inventive Principle:
Principle #3Local quality

3Productivity

If the N-type charge generation layer is doped with alkali metal or alkali earth metal, then charge generation is enhanced, but device lifetime decreases

Engineering Contradiction:
Improvecharge generationVSAvoiddevice lifetime
Core Design Contradiction:
ProductivityVSDuration of action of stationary object

Solution Approach 1:

The patent extracts and eliminates the harmful doping approach by completely avoiding the use of alkali metals and alkali earth metals in the charge generation layers. Instead, it relies on undoped organic compounds with inherently suitable energy levels, thereby preventing the lifetime degradation caused by metal doping while maintaining effective charge generation

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent replaces the unstable doped structure with stable undoped organic compounds that have appropriate energy levels. The use of stable organic materials like TCTA, TAPC, BCP, and TPBi eliminates the need for unstable metal dopants, achieving durable charge generation without the lifetime penalty of doping

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

4Stability of the object's composition

If there is a difference in LUMO energy level between the P-type charge generation layer and the N-type charge generation layer, then charge distribution is achieved, but electron injection into the N-type charge generation layer deteriorates

Engineering Contradiction:
Improvecharge distributionVSAvoidelectron injection
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

The patent carefully adjusts the LUMO energy level parameter of the P-type CGL and the HOMO energy level parameter of the N-type CGL to create an intermediate energy level梯度的 interface. By selecting P-type materials with LUMO levels of 2.5-3.5 eV and N-type materials with HOMO levels of 5.5-6.0 eV, the patent ensures smooth electron injection while maintaining charge distribution

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces an intermediate energy level structure at the interface between the P-type and N-type charge generation layers. The overlapping energy level ranges create a transitional region that facilitates electron injection from the P-type CGL to the N-type CGL, acting as an energy level intermediary that resolves the contradiction between charge distribution and injection efficiency

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of a pyrimidine derivative as an electron transport layer decreases operating voltage, increases emission efficiency, and enhances external quantum efficiency, as demonstrated by comparative examples showing reduced voltage and improved performance metrics.

Implementation Method 1

at least one among the electron transport layers in the at least two light emitting parts includes a compound represented by the following Chemical Formula 1

Methodology Applied
Scientific EffectElectron transport: Conduction (electrical)

Implementation Method 2

the difference in LUMO (lowest unoccupied molecular orbital) energy level between the P-type charge generation layer and the N-type charge generation layer deteriorates the property of injecting electrons generated at the interface

Methodology Applied
Scientific EffectElectron injection: Electron Beam

Implementation Method 3

the OLED devices are a type of devices that emit light as electrons and holes are paired and extinguished, when a charge is injected into an organic light emitting layer between an anode and a cathode

Methodology Applied
Scientific EffectElectroluminescence: Electroluminescence

Implementation Method 4

a second light emitting part using a yellow phosphorescent diode as a light emitting layer. Such a white OLED device produces white light by mixing blue light emitted from the blue fluorescent diode and yellow light emitted from the yellow phosphorescent diode

Methodology Applied
Scientific EffectPhosphorescence: Phosphorescence

Data Source

PatentEP3024050B1Organic light emitting display device
Publication Date: 2020.08.12 LG DISPLAY CO LTD
  • EP3024050B1 patent drawingFigure 1
  • EP3024050B1 patent drawingFigure 2
  • EP3024050B1 patent drawingFigure 3~4

AI summary

An organic light emitting display device is disclosed. The organic light emitting display device comprises at least two light emitting parts (ST1, ST2)between an anode (110) and a cathode (220), each of the light emitting parts having a light emitting layer (140, 190) and an electron transport layer (150, 200), charge generation layers (160N, 160P) between the at least two light emitting parts, wherein at least one among the electron transport layers in the at least two light emitting parts includes a pyrimidine derivative at both sides of the core so as to reduce a driving voltage and increase an efficiency of the organic light emitting display device.