qPCR Normalization Using Quenching Primers for Multiplex Detection

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Solution Overview

Problem

Existing qPCR methods face challenges in accurately quantifying nucleic acids due to skewed reaction efficiency and the presence of inhibitors, leading to over- or under-quantitation, and are limited in simultaneously amplifying multiple targets using intercalating dyes.

Innovation Solution

The use of fluorescence quenching primers with multiple quenchers positioned within the primer to quench the fluorescence of control nucleic acid amplicons, combined with a detectable probe that emits a distinguishable signal, allows for simultaneous amplification and detection of multiple targets in the same reaction well.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If fluorescent DNA intercalators are used to detect amplification products, then fluorescence signal is generated for quantitation, but skewed reaction efficiency and inhibitors cause over- or under-quantitation

Engineering Contradiction:
Improvequantitation accuracyVSAvoidreaction efficiency consistency
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

A control nucleic acid with a distinguishable sequence is introduced as an intermediary standard. This control serves as a reference that is amplified alongside the target nucleic acid, allowing normalization of fluorescence signals to account for variations in reaction efficiency and inhibitor effects, thereby improving quantitation accuracy

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention changes the detection parameter by using differential fluorescence detection. The control nucleic acid is detected at a first wavelength and the target nucleic acid at a second wavelength, allowing separate quantitation that can be normalized to correct for reaction variability

Inventive Principle:
Principle #35Parameter changes

2Productivity

If multiple targets are amplified simultaneously using intercalating dyes, then productivity increases, but fluorescence signals from multiple targets cannot be distinguished

Engineering Contradiction:
Improveamplification throughputVSAvoidsignal differentiation
Core Design Contradiction:
ProductivityVSDifficulty of detecting and measuring

Solution Approach 1:

The invention applies local quality by assigning different detection wavelengths to different nucleic acid targets. The control nucleic acid is detected at a first wavelength while the target nucleic acid is detected at a second wavelength, allowing simultaneous amplification and distinct detection of multiple targets in the same reaction well

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The fluorescent DNA intercalator serves multiple functions by binding to and enabling detection of both control and target nucleic acids simultaneously. A single intercalating dye performs the function of detecting multiple different nucleic acid sequences through wavelength differentiation, eliminating the need for multiple different dyes

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables accurate normalization of qPCR results by quenching excess fluorescence, allowing for concurrent amplification and detection of multiple targets with improved quantitation accuracy and efficiency.

Implementation Method 1

each of the forward quenching primer and the reverse quenching primer comprises two or more quenchers and wherein the two or more quenchers are positioned within the primer such that the quenchers quench all or substantially all of the fluorescence from an amplification product of the control nucleic acid

Methodology Applied
Scientific EffectFluorescence quenching: Fluorescence

Implementation Method 2

fluorescence emitted by a fluorescent DNA intercalator bound to the amplification product of the control nucleic acid

Methodology Applied
Scientific EffectFluorescence: Fluorescence

Data Source

PatentEP3765479B1Quantitative amplification normalization with quenchers
Publication Date: 2025.11.26 BIO RAD LABORATORIES INC
  • EP3765479B1 patent drawingFigure 1
  • EP3765479B1 patent drawingFigure 2A~2B
  • EP3765479B1 patent drawingFigure 3A

AI summary

Compositions, kits, and methods are provided for the normalization of a quantitative polymerase chain reaction (PCR) amplification. Also provided are compositions, kits, and methods for multiplexing qPCR amplification of two or more target nucleic acids in the same well.