Radiometric Density Calibration via Empty Container Attenuation

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current radiometric density measurement methods require extensive calibration efforts, often involving significant quantities of calibration media and are not very reliable due to geometric influences, leading to reduced measurement accuracy.

Innovation Solution

A single-point calibration method for radiometric density measuring devices, where the count rate of gamma radiation passing through an empty container is determined to calculate the mass attenuation coefficient, allowing for a calibration curve to be established with minimal experimental effort and improved accuracy.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If a two-point calibration method is used with media of known densities, then the mass attenuation coefficient can be determined, but the calibration process becomes complex and requires significant quantities of calibration media

Engineering Contradiction:
Improvedetermination of mass attenuation coefficientVSAvoidcalibration process complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The invention extracts the container wall attenuation effect from the overall measurement system. By separately measuring and quantifying the attenuation caused by the container wall using a radiation source and detector, this attenuation component is removed from the calibration complexity. The method determines wall attenuation by measuring radiation intensity with an empty container and calculating the attenuation coefficient specific to the wall material, thereby simplifying the calibration process while maintaining accuracy.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention introduces an intermediary measurement approach by using a known density medium (such as water) as a reference. This intermediary medium allows the system to first characterize the container wall attenuation separately, then use this characterization to simplify subsequent calibrations. The known density medium serves as a mediator that enables the determination of unknown medium densities without requiring multiple calibration points.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Measurement precision

If calibration is performed with multiple media of different densities, then measurement accuracy improves, but the quantity of calibration media required increases significantly

Engineering Contradiction:
Improvedensity measurement accuracyVSAvoidquantity of calibration media
Core Design Contradiction:
Measurement precisionVSQuantity of substance

Solution Approach 1:

The method extracts and separately characterizes the container wall attenuation component. By measuring radiation attenuation through the empty container and calculating the wall-specific attenuation coefficient, the system removes the need to fill the container with large quantities of various calibration media. The wall attenuation is determined once and reused, significantly reducing calibration media requirements while maintaining measurement accuracy.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention performs preliminary characterization of the container wall attenuation before actual density measurements. By pre-determining the attenuation properties of the container wall using minimal calibration media (or even just the wall itself), the system eliminates the need to repeatedly fill the container with different calibration media. This preliminary action stores the wall attenuation information for use in subsequent measurements.

Inventive Principle:
Principle #10Preliminary action

3Measurement precision

If the container is filled with calibration media for measurement, then density data can be obtained, but the high radiation intensity causes practical problems

Engineering Contradiction:
Improvedensity determinationVSAvoidradiation intensity effects
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

The method extracts the container wall attenuation effect as a separate measurable quantity. By characterizing the wall attenuation independently using radiation measurements through the empty container, the system can account for wall effects without requiring high radiation intensities that would be needed if the wall attenuation were uncertain. This extraction approach reduces the harmful radiation exposure by enabling accurate measurements with lower intensities.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention creates a computational model (copy) of the container wall attenuation characteristics. Instead of physically filling the container with calibration media to account for wall effects, the system creates a mathematical representation of the wall attenuation based on separate measurements. This computational copy allows the system to correct for wall effects in software, eliminating the need for physical calibration media and reducing radiation exposure.

Inventive Principle:
Principle #26Copying

4Device complexity

If geometric influences are not accounted for in calibration, then the calibration process is simpler, but measurement reliability decreases

Engineering Contradiction:
Improvecalibration procedureVSAvoidmeasurement reliability
Core Design Contradiction:
Device complexityVSReliability

Solution Approach 1:

The invention extracts and separately measures the geometric attenuation effects caused by the container wall. By using a radiation source and detector to measure transmission through the empty container, the system quantifies the geometric and material attenuation properties of the wall. This extracted information is then used to correct subsequent density measurements, improving reliability without significantly complicating the calibration procedure.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The system uses an intermediary measurement through the empty container to characterize geometric influences. This intermediary measurement provides data about the container geometry and wall attenuation, which then serves as a foundation for correcting actual density measurements. The intermediary step accounts for geometric effects without requiring complex multi-point calibrations, thereby improving reliability while maintaining procedural simplicity.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method significantly reduces calibration effort while maintaining measurement accuracy by using the count rate of gamma radiation through an empty container to calculate the mass attenuation coefficient, providing a reliable calibration curve for radiometric density measurements.

Implementation Method 1

the transmitting unit emits radioactive radiation of a predetermined intensity

Methodology Applied
Scientific EffectGamma radiation emission: Radioactive Decay

Implementation Method 2

The gamma radiation emitted by the transmitter unit is at least attenuated or dampened as it passes through the medium and/or container. The attenuation or dampening of the gamma radiation is functionally dependent on the density of the medium

Methodology Applied
Scientific EffectGamma radiation attenuation: Absorption (EM radiation)

Implementation Method 3

The attenuated or dampened gamma radiation strikes the detector material of the detector unit, where it is transformed into light pulses that are detected by a detector

Methodology Applied
Scientific EffectGamma radiation detection: Photoelectric Effect

Implementation Method 4

The receiving unit consists either of plastic or a crystal, a photomultiplier, and receiving elements

Methodology Applied
Scientific EffectScintillation: Scintillation

Data Source

PatentEP4067863B1Method for calibrating a radiometric density measuring device
Publication Date: 2024.11.20 ENDRESS & HAUSER GMBH & CO KG
  • EP4067863B1 patent drawingFigure 1~2
  • EP4067863B1 patent drawing
  • EP4067863B1 patent drawing

AI summary

The invention relates to a method for calibrating a radiometric device for determining and/or monitoring the density of a medium (6) located in a container (1). The method comprises the following steps: • Determining the count rate N0 of the radioactive radiation after passing through the empty container (1) based on the activity of the transmitter unit (3), • Determining the measured count rate N of the radioactive radiation after passing through the container (1) when a calibration medium of known density is located in the container (1), • Determining the mass damping coefficient (µ) according to the formula µ = -(ln(N/N0))/(ρ1D), where D: beam path of the radioactive radiation or inner diameter of the container (1), ρ1: density of the calibration medium, • Calculating a calibration curve that shows the dependence of the density of the medium on the count rate of the measured radiation intensity after passing through the container (1).