Raman Spectrometer Laser Power Calibration

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing Raman spectroscopy systems lack the ability to accurately measure and control laser power at the sample plane, relying on estimation methods that are inaccurate due to changes in laser power over time and variations in optical components' properties with different wavelengths.

Innovation Solution

A novel Raman spectrograph system that supports multiple laser wavelengths, allowing for the storage and recall of power calibration factors for interchangeable optical components, enabling precise control and display of optical power at the sample plane using nonvolatile memory devices and automated power adjustment.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If a single point calibration factor is used to estimate power at the sample, then the device complexity is reduced, but the measurement precision deteriorates because different wavelengths and optical components affect the actual applied power which is unaccounted for

Engineering Contradiction:
Improvecalibration systemVSAvoidpower measurement
Core Design Contradiction:
Device complexityVSMeasurement precision

Solution Approach 1:

The calibration system is segmented into multiple wavelength-specific calibration factors stored in a database, rather than using a single calibration factor. Each wavelength has its own calibration data, allowing the system to select the appropriate calibration factor based on the current laser wavelength, thereby improving measurement precision without excessive complexity

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Calibration data is pre-measured and stored in a database for multiple wavelengths and optical component configurations before actual use. When the system operates, it simply retrieves the pre-stored calibration factor corresponding to the current configuration, eliminating the need for real-time complex calculations while maintaining high precision

Inventive Principle:
Principle #10Preliminary action

2Reliability

If laser power is monitored continuously to track service life, then the reliability is improved, but the loss of time increases due to the need to remove the sample for measurement

Engineering Contradiction:
Improvelaser power monitoringVSAvoidmeasurement time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

A beam splitter is introduced as an intermediary element that divides the laser beam into two paths: one path continues to the sample for normal Raman measurement, while the other path is directed to a power meter for continuous power monitoring. This allows simultaneous sample analysis and power tracking without removing the sample or interrupting the measurement process

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The power monitoring system operates continuously alongside the Raman measurement process. The beam splitter enables both functions to occur simultaneously and continuously, eliminating the need to stop or pause measurements for power checks, thus maintaining uninterrupted useful action

Inventive Principle:
Principle #20Continuity of useful action

3Adaptability or versatility

If optical components are made interchangeable to improve versatility, then the adaptability is improved, but the device complexity increases due to the need for multiple calibration factors

Engineering Contradiction:
Improveoptical component interchangeabilityVSAvoidcalibration data management
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The system uses a universal database structure and control software that can manage calibration data for multiple wavelengths and optical component types through a single integrated interface. The beam splitter and power meter configuration is universal across different component combinations, allowing the system to handle various interchangeable components without requiring fundamentally different calibration approaches

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

All calibration data for interchangeable optical components is pre-measured and stored in the database with clear identification of which components and wavelengths each calibration factor applies to. When components are interchanged, the system automatically retrieves the appropriate pre-stored calibration data, eliminating the need for complex real-time calibration calculations and simplifying data management

Inventive Principle:
Principle #10Preliminary action

Data Source

PatentUS8111392B1Raman spectrometer with display of laser power at the sample
Publication Date: 2012.02.07 THERMO ELECTRONICS SCI INSTR LLC
  • US8111392B1 patent drawing
  • US8111392B1 patent drawing
  • US8111392B1 patent drawing

AI summary

A Raman optical method and apparatus is utilized to automatically and accurately recognize laser power measurements made at a desired illumination sample plane. From such a configuration, the methods and systems disclosed herein, enable the support of multiple optical wavelengths coupled with essential components, such as, but not limited to, filters, objectives, reflectors, etc., to provide the capability of displaying and controlling the optical power at the desired sample plane through storage of power calibration factors that are associated with such components. In particular, the system utilized herein, can recognize the installation of components and recalls stored calibration factors that are associated with such components to ensure an accurate power measurement at the illuminated sample plane.