Rapid Nucleic Acid Hybridization via Thermal Cycling

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Solution Overview

Problem

Current targeted next-generation sequencing technologies face significant bottlenecks in the time-consuming and costly process of selectively capturing and enriching targeted exons or intron regions scattered over genomic, mitochondria, and other forms of DNA, with conventional hybrid capture procedures often taking 16 hours to over 70 hours.

Innovation Solution

A novel hybridization method using a composition with a divalent cation salt concentration of 100 mM to 600 mM, a buffering agent, and a volume-excluding/thickening agent like hydroxypropyl methyl cellulose, allowing for rapid nucleic acid hybridization by incubating at two different temperatures, significantly reducing the enrichment time.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of time

If conventional hybrid capture procedures are used for target enrichment, then enrichment completeness is achieved, but the process takes 16 hours to over 70 hours

Engineering Contradiction:
Improvehybridization timeVSAvoidenrichment completeness
Core Design Contradiction:
Loss of timeVSReliability

Solution Approach 1:

The patent applies parameter changes by using a two-temperature cycling incubation protocol (alternating between 65°C and 37°C) instead of conventional constant temperature incubation. This temperature cycling, combined with high divalent cation concentration (100-600 mM), accelerates hybridization kinetics while maintaining enrichment completeness, reducing the process from 16-70 hours to approximately 1 hour.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention employs periodic action through two-temperature cycling incubation, where the hybridization mixture is repeatedly subjected to alternating high and low temperatures. This periodic thermal treatment enhances the hybridization rate and target enrichment efficiency, achieving complete enrichment in about 1 hour compared to the conventional 16-70 hour timeframe.

Inventive Principle:
Principle #19Periodic action

2Productivity

If high divalent cation concentration is used in the hybridization composition, then hybridization speed increases, but non-specific binding may increase

Engineering Contradiction:
Improvehybridization speedVSAvoidhybridization specificity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent utilizes parameter changes by implementing two-temperature cycling incubation in conjunction with high divalent cation concentration (100-600 mM). The alternating temperature protocol enhances hybridization kinetics to achieve rapid enrichment while the periodic thermal treatment also helps maintain specificity by allowing proper strand separation and reannealing, preventing non-specific binding despite the high cation concentration.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enables rapid target enrichment of genomic DNA, completing the hybridization process in as little as 1 hour, thereby speeding up the entire targeted next-generation sequencing process and improving efficiency and cost-effectiveness.

Implementation Method 1

a method for nucleic acid hybridization of a target nucleic acid and a bait nucleic acid, comprising contacting a target nucleic acid and a bait nucleic acid with a composition to form a hybridization mixture

Methodology Applied
Scientific EffectHybridization:

Implementation Method 2

a volume-excluding/thickening agent that has a concentration in a range from 0.002% to 0.1%, and wherein the volume-excluding/thickening agent is selected from the group consisting of hydroxypropyl methyl cellulose (HPMC) and methyl cellulose

Methodology Applied
Scientific EffectVolume-excluding effect:

Implementation Method 3

incubating the mixture at two hybridization temperatures, which can be different or the same

Methodology Applied
Scientific EffectThermal cycling:

Data Source

PatentEP3252172B1Fast hybridization for next generation sequencing target enrichment
Publication Date: 2024.09.11 AGILENT TECHNOLOGIES INC
  • EP3252172B1 patent drawingFigure 1
  • EP3252172B1 patent drawingFigure 2
  • EP3252172B1 patent drawingFigure 3

AI summary

The present invention relates to compositions and methods of target enrichment or selection of nucleic acids using hybridization, which can be used in, e.g., next-generation sequencing.