Raw Material Gas Heating Control for Stable CVD Film Growth

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Solution Overview

Problem

Existing methods for controlling the flow rate of raw material gas in chemical vapor deposition (CVD) processes face challenges in maintaining a consistent film formation rate as the amount of solid raw material decreases, leading to inefficiencies and variations in film thickness.

Innovation Solution

A method that adjusts the power supplied to heaters in the raw material container based on a predefined relationship with an index value corresponding to the remaining amount of solid raw material, ensuring consistent sublimation and film formation rate by dynamically correcting the heater power as the raw material depletes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If the heater power is kept constant during the CVD process, then the initial film formation rate is maintained, but the film formation rate decreases as the solid raw material depletes

Engineering Contradiction:
Improvefilm thickness consistencyVSAvoidfilm formation rate
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The heater power is made dynamic rather than constant. The power supply to the heater is adjusted in real-time based on the remaining amount of solid raw material in the container. As the raw material depletes, the heater power is increased to compensate for reduced heat capacity, maintaining consistent sublimation rate and film formation rate throughout the process.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The physical parameter being changed is the heater power (energy input). The system monitors the remaining raw material amount and相应ly adjusts the heater power parameter to maintain optimal sublimation conditions. This parameter adjustment compensates for the changing thermal environment as raw material is consumed.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If the heater power is increased to maintain film formation rate, then productivity is maintained, but energy consumption increases

Engineering Contradiction:
Improvefilm formation rateVSAvoidheater power consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The system implements feedback control by monitoring the remaining amount of solid raw material and using this information to adjust the heater power. The feedback mechanism ensures that power is increased only when necessary (when raw material depletes) and maintains optimal levels when raw material is abundant, preventing unnecessary energy consumption while ensuring productivity when needed.

Inventive Principle:
Principle #23Feedback

3Manufacturing precision

If the heater power is adjusted dynamically, then film formation rate consistency is improved, but control system complexity increases

Engineering Contradiction:
Improvefilm thickness consistencyVSAvoidcontrol system complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The system achieves self-service by automatically monitoring its own state (remaining raw material amount) and self-adjusting the heater power accordingly. This eliminates the need for complex external control systems or manual intervention, as the system autonomously maintains optimal conditions based on its internal state.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach maintains a stable film formation rate by compensating for changes in the heat capacity of the raw material container, thereby ensuring consistent film thickness and process efficiency.

Implementation Method 1

heating an inside of the raw material container to sublimate the solid raw material

Methodology Applied
Scientific EffectSublimation: Sublimation

Implementation Method 2

supplying a power to at least one heater provided at a raw material container and heating an inside of the raw material container

Methodology Applied
Scientific EffectJoule heating: Joule Heating

Data Source

PatentUS20260062801A1Method of supplying raw material gas, apparatus for supplying raw material gas, and apparatus for forming film on substrate
Publication Date: 2026.03.05 TOKYO ELECTRON LTD
  • US20260062801A1 patent drawing
  • US20260062801A1 patent drawing
  • US20260062801A1 patent drawing

AI summary

A method of supplying a raw material gas includes: supplying a power to at least one heater provided at a raw material container in which a solid raw material is accommodated and heating an inside of the raw material container to sublimate the solid raw material; supplying a carrier gas to the raw material container being heated by the heater and mixing the carrier gas with the sublimated solid raw material to supply a mixed gas as the raw material gas to a consumption zone in which a substrate is disposed; and acquiring an index value having a corresponding relationship with a remaining amount of the solid raw material, wherein, in sublimating the solid raw material, a power corresponding to the index value is supplied to the heater, based on a corresponding relationship between the index value, which is preset, and the power supplied to the heater.