Reactive Metal Powder Atomization Using Additive Gas for Flowability

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Solution Overview

Problem

Reactive metal powders often exhibit poor flowability due to static electricity sensitivity, leading to agglomeration, pipe clogging, and difficulty in sieving, which is detrimental for applications like 3D printing and coatings.

Innovation Solution

A process involving the contact of a heated metal source with at least one additive gas during atomization to produce reactive metal powders with improved flowability, achieving specific particle size distributions and reduced electronegative atom/molecule content.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional atomization process is used without additive gas, then production process is simple, but powder flowability is poor and agglomeration occurs

Engineering Contradiction:
Improveprocess simplicityVSAvoidpowder flowability
Core Design Contradiction:
Ease of manufactureVSEase of operation

Solution Approach 1:

An additive gas is introduced as an intermediary substance during the atomization process to modify the powder surface properties. The gas interacts with the molten metal droplets to create a surface layer that reduces electrostatic charge accumulation, thereby improving flowability without complicating the overall manufacturing process

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The chemical composition of the atomization atmosphere is changed by adding specific gases. This parameter change affects the surface chemistry of the formed powder particles, reducing their tendency to agglomerate and improving flow characteristics while maintaining process simplicity

Inventive Principle:
Principle #35Parameter changes

2Loss of time

If conventional atomization process is used without additive gas, then processing time is short, but powder exhibits static electricity sensitivity causing handling problems

Engineering Contradiction:
Improveprocessing timeVSAvoidstatic electricity sensitivity
Core Design Contradiction:
Loss of timeVSObject-affected harmful factors

Solution Approach 1:

The additive gas serves as a mediator that reduces static electricity sensitivity during the atomization process itself, eliminating the need for additional post-processing steps to mitigate electrostatic issues. This maintains short processing time while resolving the harmful static electricity effects

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The additive gas is introduced during atomization to preliminarily address static electricity sensitivity before the powder is formed and handled. This preliminary action prevents agglomeration and handling problems from the outset, avoiding the need for additional processing time

Inventive Principle:
Principle #10Preliminary action

3Ease of operation

If additive gas is contacted with heated metal source during atomization, then powder flowability is improved, but process complexity increases

Engineering Contradiction:
Improvepowder flowabilityVSAvoidprocess complexity
Core Design Contradiction:
Ease of operationVSDevice complexity

Solution Approach 1:

The additive gas serves multiple functions simultaneously: it modifies surface chemistry to improve flowability, reduces static electricity sensitivity, and prevents agglomeration. This multi-functionality justifies the added process complexity by addressing multiple problems with a single intervention

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The additive gas acts as a versatile intermediary that accomplishes multiple objectives during the atomization process, making the increased process complexity worthwhile by simultaneously improving flowability, reducing static sensitivity, and preventing agglomeration

Inventive Principle:
Principle #24Intermediary (Mediator)

4Manufacturing precision

If additive gas is used during atomization, then uniform layer formation is enabled, but gas mixing complexity increases

Engineering Contradiction:
Improveuniform layer formationVSAvoidgas mixing complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The composition of the atomization atmosphere is precisely controlled by adjusting the ratio and type of additive gas. This parameter control enables uniform layer formation by ensuring consistent powder flow and distribution characteristics, justifying the gas mixing complexity through improved manufacturing precision

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process enhances flowability of reactive metal powders, reducing static electricity sensitivity and enabling uniform layer formation, thus improving their suitability for applications such as powder metallurgy and coatings.

Implementation Method 1

contacting said heated metal source with at least one additive gas while carrying out said atomization process

Methodology Applied
Scientific EffectAtomization:

Data Source

PatentEP4640343A1Metal powder atomization manufacturing processes
Publication Date: 2025.10.29 AP&C ADVANCED POWDERS & COATINGS
  • EP4640343A1 patent drawingFigure 1
  • EP4640343A1 patent drawingFigure 2
  • EP4640343A1 patent drawingFigure 3

AI summary

There are provided reactive metal powder atomization manufacturing processes. For example, such processes include providing a heated metal source and contact the heated metal source with at least one additive gas while carrying out the atomization process. Such processes provide raw reactive metal powder having improved flowability. The at least one additive gas can be mixed together with an atomization gas to obtain an atomization mixture, and the heated metal source can be contacted with the atomization mixture while carrying out the atomization process. Reactive metal powder spheroidization manufacturing processes are also provided.