Continuous Mixing Reactor Flow Distribution and Tube Wear

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Solution Overview

Problem

Conventional continuous mixing reactors experience tube wear and uneven flow distribution in the reversal area, leading to pressure losses and inefficient heat exchange in the tube bundle, particularly in acid-catalyst alkylation processes.

Innovation Solution

The reactor design features a cylindrical shell with conical end sections and a tangentially terminating circulation tube, along with a flow distribution plate, to enhance fluid flow and heat exchange efficiency, reducing tube wear and improving flow distribution within the tube bundle.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If a conventional flow path with a circulation tube is used in a continuous mixing reactor, then mixing and circulation are achieved, but tube wear occurs in the reversal area and flow distribution becomes uneven

Engineering Contradiction:
Improvemixing and circulationVSAvoidtube wear
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The circulation tube is divided into multiple sections with different diameters - a larger diameter section near the impeller and a smaller diameter section extending toward the discharge. This segmentation allows optimization of flow characteristics in different zones, reducing turbulence and wear in the reversal area while maintaining effective mixing near the impeller.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different sections of the circulation tube are given different properties - the larger diameter portion handles high-velocity mixed fluid from the impeller, while the smaller diameter portion manages the reversal and return flow. This local differentiation of tube dimensions addresses the specific flow conditions and wear risks in each zone.

Inventive Principle:
Principle #3Local quality

2Ease of operation

If a conventional flow path is used in a continuous mixing reactor, then circulation is established, but pressure losses occur and flow distribution to the tube bundle becomes uneven

Engineering Contradiction:
ImprovecirculationVSAvoidpressure losses
Core Design Contradiction:
Ease of operationVSLoss of energy

Solution Approach 1:

The circulation tube design creates dynamic flow control by using the larger diameter section to accommodate high-velocity flow from the impeller discharge, then transitioning to a smaller diameter section that manages the reversal flow. This dynamic adaptation to flow conditions reduces pressure losses compared to a uniform diameter tube.

Inventive Principle:
Principle #15Dynamics

3Ease of operation

If the circulation tube extends fully to the discharge end of the reactor, then flow path is established, but stagnant areas are created and heat exchange efficiency decreases

Engineering Contradiction:
Improveflow pathVSAvoidheat exchange efficiency
Core Design Contradiction:
Ease of operationVSProductivity

Solution Approach 1:

The circulation tube is intentionally not extended to the full discharge end of the reactor. Instead, it terminates at an optimal position where the smaller diameter section ends, extracting the tube from the stagnant zone near the discharge. This prevents formation of dead zones while maintaining effective circulation and heat exchange in the active reaction zone.

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design reduces tube wear, enhances heat transfer efficiency, and improves flow distribution, leading to better management of reaction temperature and reduced stagnant areas for side reactions in alkylation processes.

Implementation Method 1

The impeller effects mixing and circulation in the reactor. A mixing circulating impeller provides high shear and turbulence to reactants to maximize rate.

Methodology Applied
Scientific EffectTurbulence: Turbulence

Implementation Method 2

A mixing circulating impeller provides high shear and turbulence to reactants to maximize rate.

Methodology Applied
Scientific EffectShear: Shear Stress

Implementation Method 3

Indirect heat exchanging means provided as a tube bundle containing a heat exchanging medium for addition or removal of heat absorbed or generated during the reaction. Temperature control is achieved by addition or removal of reaction heat by heat exchange throughout a reaction zone in the reactor.

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Data Source

PatentUS10077219B2Continuous mixing reactor and method of use
Publication Date: 2018.09.18 REFINING TECHNOLOGY SOLUTIONS LLC
  • US10077219B2 patent drawing
  • US10077219B2 patent drawing
  • US10077219B2 patent drawing

AI summary

A continuous mixing reactor has an outer shell having a cylindrical portion with a central section and two opposite conical end sections; a circulation tube within the shell so that an annular passage forms between the shell and the circulation tube; an impeller within and positioned adjacent to one end of the circulation tube; and heat exchange means penetrating the outer shell and extending into the end of the circulation tube opposite the impeller. The outer shell has a hydraulic head forming one end of the shell, a heat exchange medium header at the opposite end of the shell. The circulation tube nearer the heat exchange medium header terminates at or downstream from a tangential plane extending through the shell at the intersection of the central section and the conical end section of the cylindrical portion of shell. The reactor is useful in an alkylation process.