Bubble Column Reactor Gas Distributor with Caps

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Solution Overview

Problem

Bubble column reactors face issues with non-uniform reactant distribution, dead zones, and improper mixing due to inadequate gas distributor design, affecting conversion levels and product selectivity in slurry hydrocracking of heavy oils.

Innovation Solution

A bubble column reactor assembly featuring a pre-distributor plate with caps and a helical gas distributor that breaks large gas bubbles into smaller ones, ensuring uniform gas and liquid distribution, enhanced mixing, and improved heat and mass transfer, preventing catalyst attrition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If a conventional gas distributor is used in a bubble column reactor, then the structure is simple, but non-uniform reactant distribution and dead zones occur

Engineering Contradiction:
Improveuniformity of reactant distributionVSAvoidcomplexity of gas distributor structure
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The gas distributor is segmented into multiple functional layers: a pre-distributor plate with perforations and caps, and a secondary distributor with additional perforations. This segmentation allows progressive gas distribution and bubble size control, achieving uniform reactant distribution without creating dead zones while maintaining manageable structural complexity through modular design.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Caps are introduced as intermediary elements that enclose the ends of ducts projecting from the pre-distributor plate. These caps act as mediators that further subdivide gas bubbles and facilitate uniform gas-liquid mixing, improving distribution uniformity while adding only moderate structural complexity.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of operation

If large gas bubbles are used, then the gas distributor design is simple, but improper mixing and dead zones are created

Engineering Contradiction:
Improvemixing efficiencyVSAvoidcomplexity of gas distribution system
Core Design Contradiction:
Ease of operationVSDevice complexity

Solution Approach 1:

The gas distribution system is divided into multiple stages: initial gas introduction through the pre-distributor plate, followed by further subdivision through caps on ducts, and final distribution through the secondary distributor. This multi-stage segmentation progressively breaks down large bubbles into smaller, more uniformly distributed bubbles, achieving proper mixing without requiring overly complex single-stage designs.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The pre-distributor plate with caps performs preliminary gas bubble subdivision before the gas reaches the main reaction zone. By pre-breaking large bubbles into smaller ones at the source, the system ensures improved mixing efficiency downstream while avoiding the need for complex agitation or redistribution mechanisms.

Inventive Principle:
Principle #10Preliminary action

3Productivity

If inadequate gas distribution is used, then the device structure is simple, but conversion levels and product selectivity are affected

Engineering Contradiction:
Improveconversion levelVSAvoidcomplexity of distributor design
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The distributor is segmented into functional zones: a pre-distributor plate for initial gas distribution and bubble subdivision, caps for intermediate processing, and a secondary distributor for final uniform distribution. This segmentation ensures high conversion levels through improved gas-liquid contact efficiency while maintaining reasonable structural complexity through systematic modular organization.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different regions of the gas distributor are designed with locally optimized characteristics: the pre-distributor plate provides coarse distribution, caps provide intermediate subdivision, and the secondary distributor provides fine uniform distribution. This local quality optimization ensures high productivity across the entire reactor volume without requiring uniformly complex design throughout.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves optimal gas and liquid distribution, eliminates dead zones, and enhances mass transfer rates, leading to higher conversion and product selectivity in slurry hydrocracking reactions.

Implementation Method 1

A bubble column reactor assembly featuring a pre-distributor plate with caps and a helical gas distributor that breaks large gas bubbles into smaller ones

Methodology Applied
Scientific EffectBubble breakup: Plateau-Rayleigh Instability

Implementation Method 2

ensuring uniform gas and liquid distribution, enhanced mixing, and improved heat and mass transfer

Methodology Applied
Scientific EffectGas-liquid mixing: Turbulence

Implementation Method 3

enhances mass transfer rates, leading to higher conversion and product selectivity in slurry hydrocracking reactions

Methodology Applied
Scientific EffectMass transfer: Diffusion

Data Source

PatentUS11896970B2Gas and liquid distributor for bubble column reactor
Publication Date: 2024.02.13 HINDUSTAN PETROLEUM CORP LTD
  • US11896970B2 patent drawing
  • US11896970B2 patent drawing

AI summary

Bubble column reactor assembly (100) is provided, the assembly comprising: a reactor vessel (104) comprising a bottom end and a top end; a pre-distributor plate (150) disposed above the bottom end of the reactor vessel (104) to distribute gas in a liquid, the plate comprising a bottom surface facing the bottom end of the reactor vessel (104) and a top surface opposite to the bottom surface. The pre-distributor plate (150) comprises a plurality of perforations (206), each perforation (206) comprising: a duct (170) projecting from the bottom surface of the pre-distributor plate; and a cap (180) enclosing the duct (170) and the perforation (206). The cap (180) comprises a plurality of openings (210). A gas distributor (110) is disposed below the pre-distributor plate (150) to receive gas and inject gas into the liquid prior to distribution of gas and the liquid by the pre-distributor plate (150).