Multiple-bed Downflow Reactor Mixing Device for Temperature Homogeneity

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Solution Overview

Problem

Multiple-bed downflow reactors face challenges in achieving uniform distribution of liquid and gas, leading to uneven reaction and temperature distribution across reaction beds, which affects process efficiency in hydrocarbon processing.

Innovation Solution

A mixing device with a loop of first nozzles directed inwardly and a loop of second nozzles directed outwardly around a vertical axis, where the ejection directions are defined by orthogonal vectors, promoting opposite circumferential directions to enhance mixing and reduce vertical height requirements, allowing for more homogeneous temperature distribution.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If a conventional mixing device with single-direction nozzles is used, then the device structure is simple, but the temperature distribution uniformity deteriorates

Engineering Contradiction:
Improvetemperature distribution uniformityVSAvoidmixing device structure
Core Design Contradiction:
Stability of the object's compositionVSDevice complexity

Solution Approach 1:

The mixing device is segmented into multiple nozzle loops (first loop, second loop, third loop) with different ejection directions. Each loop handles a specific directional component of the fluid mixture, dividing the complex mixing task into manageable segments that collectively achieve uniform temperature distribution.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different nozzle loops are positioned and oriented to address specific local mixing requirements within the inter-bed space. The first loop targets radial mixing, the second loop addresses tangential mixing, and the third loop handles axial mixing, ensuring that each region receives appropriate mixing intensity and direction.

Inventive Principle:
Principle #3Local quality

2Productivity

If the inter-bed vertical height is reduced by 20-40%, then reactor productivity increases, but the mixing effectiveness deteriorates

Engineering Contradiction:
Improvereactor throughputVSAvoidmixing effectiveness
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The mixing device utilizes three-dimensional nozzle arrangements with components in radial, tangential, and axial directions. This multi-dimensional approach to fluid ejection ensures effective mixing is achieved within a compressed vertical space, maintaining mixing quality while reducing the inter-bed height.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Solution Approach 2:

The mixing device creates dynamic fluid motion through multiple ejection directions and utilizes the natural downward flow of liquid from the upper bed. The combination of injected gas/liquid from nozzles and the descending liquid creates turbulent mixing that is effective in reduced vertical distances.

Inventive Principle:
Principle #15Dynamics

3Stability of the object's composition

If multiple nozzle loops with different ejection directions are added, then the temperature homogeneity improves, but the device complexity increases

Engineering Contradiction:
Improvetemperature homogeneityVSAvoidnozzle configuration
Core Design Contradiction:
Stability of the object's compositionVSDevice complexity

Solution Approach 1:

The multiple nozzle loops serve universal mixing functions despite their different orientations. All loops work together to achieve the same overall goal of temperature homogenization, with each loop contributing a specific directional component to the mixed fluid stream.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The first, second, and third nozzle loops are merged into a single integrated mixing device assembly. Their combined effect creates comprehensive three-dimensional mixing action, merging their individual contributions to achieve superior temperature homogeneity that neither loop could accomplish alone.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration increases reactor performance by reducing the vertical height of inter bed spaces by 20-40%, enabling more beds or increased performance, with improved temperature homogeneity and reduced standard deviation of temperature across the reactor.

Implementation Method 1

promoting opposite circumferential directions to enhance mixing

Methodology Applied
Scientific EffectTurbulence: Turbulence

Implementation Method 2

a loop of first nozzles distributed around a vertical axis and arranged for ejecting a fluid in a first ejection direction

Methodology Applied
Scientific EffectFluid Spray: Fluid Spray

Implementation Method 3

a swirler, which swirler is located above the collecting tray around the central gas passage, and is provided with vanes defining a swirl direction and being arranged to impart a swirling motion to gas passing through the central gas passage

Methodology Applied
Scientific EffectSwirl flow: Vortex Ring

Data Source

PatentUS10076736B2Multiple-bed downflow reactor comprising a mixing device, use of said reactor, as well as mixing method
Publication Date: 2018.09.18 SHELL USA INC
  • US10076736B2 patent drawing
  • US10076736B2 patent drawing
  • US10076736B2 patent drawing

AI summary

The present invention relates to a multiple-bed downflow reactor comprising vertically spaced beds of solid contact material and a mixing device positioned in an inter bed space between adjacent beds. The mixing device comprises a loop of first nozzles distributed around a vertical axis and arranged for ejecting a fluid in a first ejection direction into said inter bed space, on the one hand, and a loop of second nozzles distributed around the vertical axis and arranged for ejecting a fluid in a second ejection direction into said inter bed space, on the other hand. The first ejection direction is directed inwardly with respect to the loop of first nozzles. The second ejection direction is directed outwardly with respect to the loop of second nozzles.