Oxidation Reactor Refractory Lining Thermal Expansion Management

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Solution Overview

Problem

Existing oxidation reactors for partial oxidation of hydrocarbon streams suffer from thermal expansion and contraction issues, which can lead to mechanical tensions and potential damage to the fireproof bricks, compromising the reactor's integrity.

Innovation Solution

The design incorporates a multi-layered fireproof lining with ring-shaped expansion gaps and periodic empty joints to accommodate thermal expansion and contraction, preventing mechanical tensions and maintaining the structural integrity of the fireproof bricks.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a continuous fireproof brick lining is used in the oxidation reactor, then the protective function against high temperatures is improved, but thermal expansion and contraction cause mechanical tensions and potential damage to the bricks

Engineering Contradiction:
Improveprotective functionVSAvoidmechanical integrity
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The continuous fireproof brick lining is segmented by introducing ring-shaped expansion gaps at regular intervals along the reactor length. This divides the rigid lining into separate sections that can independently expand and contract thermally, eliminating cumulative mechanical tensions while maintaining protective coverage through periodic segmentation.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Ring-shaped expansion gaps are extracted from the continuous brick lining structure, creating periodic voids or reduced-density zones. These extracted sections serve as expansion compartments that accommodate thermal dimension changes, preventing stress accumulation in the remaining brick sections while preserving the overall protective function.

Inventive Principle:
Principle #2Taking out (Extraction)

2Productivity

If the oxidation reactor operates at high temperatures (1000-1500 °C) for efficient partial oxidation, then the reaction efficiency is improved, but thermal expansion and contraction of fireproof bricks increase, leading to mechanical damage

Engineering Contradiction:
Improvereaction efficiencyVSAvoidbrick integrity
Core Design Contradiction:
ProductivityVSStrength

Solution Approach 1:

The design explicitly incorporates thermal expansion gaps that accommodate the dimensional changes of fireproof bricks under high-temperature operation. By providing predetermined expansion space through ring-shaped gaps, the system allows bricks to expand freely at elevated temperatures without generating damaging compressive stresses, thereby enabling sustained high-temperature operation for efficient partial oxidation.

Inventive Principle:
Principle #37Thermal expansion

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design effectively minimizes mechanical tensions caused by thermal expansion and contraction, ensuring the structural integrity of the fireproof bricks and extending the lifespan of the oxidation reactor.

Implementation Method 1

The design incorporates a multi-layered fireproof lining with ring-shaped expansion gaps and periodic empty joints to accommodate thermal expansion and contraction, preventing mechanical tensions

Methodology Applied
Scientific EffectThermal expansion: Thermal Expansion

Data Source

PatentEP4541457A1Oxidation reactor for partial oxidation of a feed stream comprising a refractory protective layer
Publication Date: 2025.04.23 LAIR LIQUIDE SA POUR LETUDE & LEXPLOITATION DES PROCEDES GEORGES CLAUDE
  • EP4541457A1 patent drawingFigure 1
  • EP4541457A1 patent drawingFigure 2
  • EP4541457A1 patent drawingFigure 3

AI summary

The invention relates to an oxidation reactor for the partial oxidation of a feed stream containing an oxygen oxidant stream to a hydrogen-containing product stream. The partial oxidation can be carried out as non-catalytic partial oxidation (POX) or as autothermal reforming (ATR). Suitable feed streams include hydrocarbon-containing streams as well as streams containing ammonia. According to the invention, the oxidation reactor is provided within the pressure-bearing reactor shell with a protective layer of refractory bricks, wherein the bricks are arranged in the at least one protective layer such that the protective layer is movable in the radial direction during thermal expansion. This effectively prevents or at least minimizes the destruction of the bricks due to thermal expansion.