Rectification Column Temperature Profile Control for Binary Mixtures

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Solution Overview

Problem

Current methods for controlling the concentration of components in rectification columns are energy-intensive and require complex modeling, often relying on costly instruments or unsatisfactory temperature control due to high temperature gradients, especially when dealing with binary mixtures.

Innovation Solution

A method using temperature sensors to define a control zone and approximate the temperature profile with logistic functions, allowing for the estimation of mass transfer zones and manipulation of coolant and steam rates to achieve desired product concentrations with reduced modeling complexity and computing power.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If complex modeling and costly instruments are used for concentration control, then measurement precision is improved, but device complexity increases

Engineering Contradiction:
Improveconcentration control precisionVSAvoidmodeling complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent creates a simplified copy of the temperature profile using logistic functions instead of requiring complex physical models or expensive measurement instruments. This mathematical approximation captures the essential behavior of the rectification column without the complexity of rigorous models, enabling concentration control through temperature measurements alone

Inventive Principle:
Principle #26Copying

Solution Approach 2:

The invention replaces costly instruments and complex modeling systems with simple logistic function approximations that require minimal computational resources and physical data. This approach uses readily available temperature measurements and simple mathematical functions instead of expensive analytical instruments

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Manufacturing precision

If traditional temperature control methods are used, then concentration control is achieved, but energy consumption increases due to high temperature gradients

Engineering Contradiction:
Improveconcentration controlVSAvoidenergy consumption
Core Design Contradiction:
Manufacturing precisionVSUse of energy by moving object

Solution Approach 1:

The patent applies local quality by using logistic functions to approximate temperature profiles in different sections of the rectification column independently. This allows for localized control strategies that adapt to the specific temperature characteristics of each section, reducing the need for high energy input across the entire column while maintaining concentration control precision

Inventive Principle:
Principle #3Local quality

3Measurement precision

If rigorous models with extensive substance and apparatus data are used, then measurement precision is improved, but device complexity and data requirements increase

Engineering Contradiction:
Improveconcentration measurementVSAvoidmodel complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent creates a simplified mathematical copy of the complex physical system using logistic functions. Instead of requiring detailed knowledge of substance properties and apparatus characteristics, the logistic functions capture the essential temperature profile behavior, providing accurate concentration measurements without extensive data requirements

Inventive Principle:
Principle #26Copying

Solution Approach 2:

The invention changes the parameters used for concentration control from requiring extensive physical and chemical data to using only temperature measurements and logistic function parameters. This parameter transformation simplifies the control system while maintaining measurement precision

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach simplifies the control process, reduces energy consumption, and allows for efficient concentration control with lesser physical data requirements, making it suitable for productive systems without the need for dedicated hardware, while maintaining product purity and material balance.

Implementation Method 1

a control zone defined by temperature sensors arranged in longitudinal direction of the column is linearized with the aid of an estimate of a temperature profile

Methodology Applied
Scientific EffectTemperature measurement:

Implementation Method 2

Rectification exploits the physical principle that the concentration of the low boiler in the vapor phase is higher than in the liquid phase. By contrast with distillation, this process is repeated several times

Methodology Applied
Scientific EffectRectification: Distillation

Implementation Method 3

At each separation stage, as in the case of distillation, a respective phase equilibrium is established

Methodology Applied
Scientific EffectPhase equilibrium:

Implementation Method 4

a respective phase equilibrium is established. In the case of rectification, the substance having lower vapor pressure is called high boiler, and that having higher vapor pressure low boiler

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 5

coolant valve

Methodology Applied
Scientific EffectHeat removal: Cooling

Implementation Method 6

steam valve

Methodology Applied
Scientific EffectHeating: Heating

Data Source

PatentUS11235260B2Method for controlling a rectification column
Publication Date: 2022.02.01 COVESTRO DEUTSCHLAND AG
  • US11235260B2 patent drawing
  • US11235260B2 patent drawing

AI summary

The present invention relates to a method of controlling a concentration of a first component of a rectification column for separating a binary mixture of the first component with a second component on the basis of temperature measurements, wherein a control path defined by temperature sensors (T3, T2, T6) arranged in the longitudinal direction of the column is linearized with the aid of an estimated temperature profile, wherein a real temperature profile T*(h), determined by means of the temperature sensors, is approximated by a function T(h) in dependence on a column height h, wherein the column id divided into two sections along the column height h and the function T(h) is defined section by section on the basis, in each case, of a logistical function.