Reduction Catalyst with Quaternary Nitrogen for CO2 Conversion

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Solution Overview

Problem

Current technologies for CO2 reduction via artificial photochemical reactions have low efficiency due to interconnection resistance and require sacrificial reagents, with existing reduction catalysts not effectively utilizing light energy for high reaction efficiency.

Innovation Solution

A reduction catalyst with a charge collector and modified organic molecules containing quaternary nitrogen cations, which are chemically bound to a metal layer, enhancing CO2 reduction efficiency by promoting selective reactions with low energy consumption.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a photochemical reactor with electrodes and photocatalysts is used for CO2 reduction, then CO2 reduction reaction can occur, but solar energy conversion efficiency is very low at around 0.04% due to low energy efficiency of photocatalyst and interconnection resistance

Engineering Contradiction:
ImproveCO2 reduction efficiencyVSAvoidsolar energy conversion efficiency
Core Design Contradiction:
ProductivityVSLoss of energy

Solution Approach 1:

The invention extracts and eliminates the photocatalyst component from the photochemical reactor system. By removing the photocatalyst, the system avoids its low energy efficiency (0.04% solar energy conversion) and replaces it with a direct silicon solar cell-based electrochemical system that achieves much higher energy conversion efficiency while maintaining CO2 reduction capability.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention substitutes the photocatalyst-based photochemical reaction system with an electrochemical system using silicon solar cells. This replacement transitions from a photochemical mechanism to an electrochemical mechanism, eliminating the need for photocatalysts and achieving superior energy conversion efficiency.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Productivity

If electrodes are connected with electric wire to transfer electrons for CO2 reduction, then reduction reaction can proceed, but efficiency in extracting electricity decreases due to interconnection resistance

Engineering Contradiction:
ImproveCO2 reduction efficiencyVSAvoidelectricity extraction efficiency
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The invention merges the electron generation function (silicon solar cell) and electron consumption function (CO2 reduction reaction) into a single integrated device structure. The silicon solar cell and catalyst layers are directly combined without external wiring, eliminating interconnection resistance and achieving efficient electron transfer for CO2 reduction.

Inventive Principle:
Principle #5Merging (Combining)

3Ease of manufacture

If a plate-like laminated structure with silicon solar cell is used, then device can be easily increased in size and no wiring is required, but CO2 reduction reaction does not proceed effectively because ions need to move to opposite sides

Engineering Contradiction:
Improvedevice scalabilityVSAvoidCO2 reduction reaction efficiency
Core Design Contradiction:
Ease of manufactureVSProductivity

Solution Approach 1:

The invention applies local quality by creating distinct functional zones within the device: a catalyst layer configured to promote CO2 reduction reaction at specific locations, and an ion movement path that enables efficient ion transport. This localized functional design allows the plate-like structure to maintain both scalability and effective CO2 reduction performance.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The invention introduces an ion movement path as an intermediary component that facilitates ion transport between different regions of the device. This intermediary structure enables ions to move efficiently to the opposite sides where needed, resolving the limitation of the plate-like laminated structure while maintaining its scalability advantages.

Inventive Principle:
Principle #24Intermediary (Mediator)

4Quantity of substance

If a large number of electrons are required for CO2 reduction to produce hydrocarbons, then desired hydrocarbon can be produced, but reduction reaction becomes more difficult to advance with Faraday efficiency

Engineering Contradiction:
Improvehydrocarbon productionVSAvoidFaraday efficiency
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The invention changes the chemical and physical parameters of the catalyst layer to optimize CO2 reduction performance. By configuring specific catalyst materials and their properties, the system achieves high Faraday efficiency even for multi-electron reduction reactions that produce desired hydrocarbons, overcoming the inherent difficulty of advancing reactions requiring multiple electrons.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The catalyst achieves high CO2 reduction efficiency by increasing the reactive surface area and selectively advancing the reduction reaction with low energy input, improving Faraday efficiency and product selectivity.

Implementation Method 1

A reduction catalyst with a charge collector and modified organic molecules containing quaternary nitrogen cations, which are chemically bound to a metal layer, enhancing CO2 reduction efficiency by promoting selective reactions with low energy consumption.

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

The catalyst achieves high CO2 reduction efficiency by increasing the reactive surface area and selectively advancing the reduction reaction with low energy input, improving Faraday efficiency and product selectivity.

Methodology Applied
Scientific EffectElectron transfer:

Implementation Method 3

The electrode for reduction reaction gains a reduction potential of CO2 from the electrode for oxidation reaction to reduce CO2, and, thus, to produce formic acid (HCOOH).

Methodology Applied
Scientific EffectPhotoelectric effect: Photoelectric Effect

Data Source

PatentEP3006604B1Reduction catalyst and chemical reactor
Publication Date: 2018.12.12 KK TOSHIBA
  • EP3006604B1 patent drawingFigure 1
  • EP3006604B1 patent drawingFigure 2
  • EP3006604B1 patent drawingFigure 3~4

AI summary

According to one embodiment, a reduction catalyst includes a charge collector having a metal layer on a surface; and a modified organic molecule bound to a surface of the metal layer and containing a quaternary nitrogen cation.