Refractory Lining for Delayed Coker Drum Thermal Fatigue

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Solution Overview

Problem

Delayed coking coke drums experience thermal fatigue and pressure boundary cracking due to transient thermal stresses during the quench and heat-up phases of the coking process, leading to potential drum bulging and mechanical stress issues.

Innovation Solution

A thermal buffering system using a monolithic, thermal shock-resistant, and erosion-resistant refractory lining is applied to the internal surface of the coke drum, particularly at areas prone to pressure boundary stress, with a suitable anchoring system to dissipate thermal stresses across the lining rather than the drum's pressure boundary.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If a steel drum is used for delayed coking, then the drum can withstand high pressure and temperature, but the drum experiences thermal fatigue and pressure boundary cracking due to transient thermal stresses

Engineering Contradiction:
Improvepressure withstanding capabilityVSAvoidthermal fatigue resistance
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The patent applies a composite structure consisting of an inner refractory lining layer and an outer steel pressure boundary layer. The refractory lining (made of materials like alumina, silica, or magnesia) provides thermal shock resistance and protects the steel shell from transient thermal stresses, while the steel layer provides mechanical strength and pressure containment. This composite material approach resolves the contradiction by combining materials with complementary properties.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The refractory lining acts as an intermediary layer between the hot coke/steam environment and the steel pressure boundary. It mediates the thermal stresses by absorbing and dissipating thermal energy, preventing direct thermal shock to the steel drum. The lining serves as a buffer that protects the structural integrity of the steel shell during thermal cycling.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If the drum is subjected to rapid quenching to reduce cycle time, then productivity increases, but thermal stress and drum bulging increase

Engineering Contradiction:
Improvecoking cycle speedVSAvoidthermal stress
Core Design Contradiction:
ProductivityVSStress or pressure

Solution Approach 1:

The refractory lining is installed beforehand as a protective cushion against thermal shock. During rapid quenching operations, the lining absorbs the thermal stress impact that would otherwise directly affect the steel drum, enabling faster cycle times without proportionally increasing thermal stress on the pressure boundary. The lining is pre-positioned to cushion against anticipated thermal shocks.

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

Solution Approach 2:

The patent changes the thermal parameters of the drum system by introducing a lining with different thermal properties (lower thermal conductivity, higher thermal shock resistance) compared to bare steel. This parameter change allows the drum to withstand more aggressive quenching conditions, thereby increasing productivity without linearly increasing thermal stress on the steel structure.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If internal cladding is applied to protect against sulfur corrosion, then corrosion resistance improves, but the complexity of manufacturing and installation increases

Engineering Contradiction:
Improvecorrosion resistanceVSAvoidmanufacturing complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The refractory lining serves multiple functions simultaneously: it provides thermal shock resistance, protects against sulfur corrosion, and reduces thermal stress on the steel shell. By consolidating these protection functions into a single multi-functional lining system, the patent reduces overall system complexity compared to applying separate specialized claddings for each protection need.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The refractory lining combines protective properties against both thermal shock and chemical corrosion in a single material system. Materials like alumina-silica compositions provide both thermal stability and resistance to sulfur-containing environments, eliminating the need for separate corrosion protection layers and simplifying the overall drum construction.

Inventive Principle:
Principle #40Composite materials

4Reliability

If the drum shell thickness is increased to reduce thermal stress, then thermal fatigue resistance improves, but the drum weight and capital cost increase

Engineering Contradiction:
Improvethermal fatigue resistanceVSAvoiddrum weight
Core Design Contradiction:
ReliabilityVSWeight of moving object

Solution Approach 1:

Instead of increasing steel shell thickness to improve thermal fatigue resistance, the patent uses a composite structure with a relatively thin steel shell supported by a thick refractory lining. The refractory material (which is lighter than equivalent steel thickness) provides the thermal protection, while the steel shell maintains adequate structural strength. This composite approach reduces overall weight compared to a thick steel shell design.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The refractory lining acts as an intermediary that bears the thermal fatigue load, allowing the steel shell to remain thinner. The lining absorbs the thermal cycling stresses, so the steel pressure boundary doesn't need to be oversized for thermal protection. This mediator approach enables weight reduction while maintaining thermal fatigue resistance.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution significantly reduces thermal fatigue in the coke drum shell and minimizes skirt-to-shell cracking, allowing for shorter quench phases and reduced cycle times, potentially eliminating the need for internal cladding and reducing erosion from high-pressure cutting water, while maintaining refractory integrity through coke impregnation.

Implementation Method 1

A thermal buffering system using a monolithic, thermal shock-resistant, and erosion-resistant refractory lining is applied to the internal surface of the coke drum... to dissipate thermal stresses across the lining rather than the drum's pressure boundary

Methodology Applied
Scientific EffectThermal insulation: Thermal Insulation

Implementation Method 2

A thermal buffering system using a monolithic, thermal shock-resistant, and erosion-resistant refractory lining is applied to the internal surface of the coke drum

Methodology Applied
Scientific EffectThermal shock resistance: Thermal Shock

Implementation Method 3

maintaining refractory integrity through coke impregnation

Methodology Applied
Scientific EffectImpregnation: Absorption (physical)

Data Source

PatentEP3116976B1Internal lining for delayed coker drum
Publication Date: 2020.11.04 EXXONMOBIL TECHNOLOGY & ENGINEERING CO
  • EP3116976B1 patent drawingFigure 1
  • EP3116976B1 patent drawingFigure 2
  • EP3116976B1 patent drawingFigure 3

AI summary

A delayed coking unit has a thermal shock-resistant, erosion-resistant internal lining to reduce thermally-induced mechanical stresses in the pressure boundary of the coke drum. The lining is effective to reduce or mitigate the transient thermal stress that occurs in the pressure boundary of the coke drum and to reduce or minimize the high thermal stress resulting from temperature differentials at the skirt-to-shell junction.