Remote Polarimeter Sample Cell Filling Device

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Solution Overview

Problem

Existing polarimeter sample cell filling methods are incompatible with modern laboratory safety practices, as they often require bubble detection near the instrument, which can lead to contamination or damage, and traditional methods are inefficient for verifying proper filling away from the polarimeter.

Innovation Solution

A sample cell filling device with a liquid-sealed housing, light source, and diffuser viewing screen allows remote filling verification by observing light changes through the viewing screen, indicating bubble presence or absence, facilitating safe and convenient filling at a workbench or under a fume hood.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If bubble detection is performed near the polarimeter using traditional eye methods or built-in camera, then bubble detection can be performed, but laboratory safety is compromised and contamination or damage may occur

Engineering Contradiction:
Improvebubble detection capabilityVSAvoidcontamination and damage risk
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The device separates the bubble detection function from the polarimeter by providing a standalone viewing device with a viewing chamber. This allows operators to perform bubble detection in a separate, safer location (preparation area) rather than near the polarimeter instrument, thus eliminating contamination and damage risks while maintaining detection capability.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The viewing device acts as an intermediary between the sample cell filling process and the polarimeter. It provides a remote observation point where bubbles can be detected through the viewing chamber without requiring the operator to be in close proximity to the polarimeter or handle uncapped sample cells near the instrument.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Object-affected harmful factors

If sample cells are filled and inspected at the preparation area away from the polarimeter, then safety is improved, but traditional eye methods are inefficient and require uncapped cells near the face

Engineering Contradiction:
Improvesafety from contaminationVSAvoidfilling verification efficiency
Core Design Contradiction:
Object-affected harmful factorsVSEase of operation

Solution Approach 1:

The device replaces the traditional mechanical eye-based inspection method with an optical system consisting of a light source, viewing chamber, and viewing screen. This allows efficient bubble detection at workbench height or under fume hoods without requiring operators to incline cells toward light sources or risk spilling hazardous materials near their faces.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The viewing screen displays optical characteristics (brightness, uniformity) that change based on the presence or absence of bubbles in the sample cell. This provides clear visual feedback to operators about fill quality without requiring direct observation through the sample cell itself, improving both safety and efficiency.

Inventive Principle:
Principle #32Color changes

3Extent of automation

If built-in camera is used for bubble detection, then automated detection is achieved, but detection occurs too late when samples arrive at the instrument

Engineering Contradiction:
Improveautomated bubble detectionVSAvoiddetection timing
Core Design Contradiction:
Extent of automationVSLoss of time

Solution Approach 1:

The viewing device enables bubble detection to be performed in advance, before the sample cell is delivered to the polarimeter. Operators can inspect filled cells at the preparation area while they are still accessible, eliminating the need to wait until samples arrive at the instrument and allowing immediate correction of fill defects.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The device enables safe and efficient bubble detection and spill reduction, promoting proper filling techniques and easy decontamination, ensuring accurate sample cell filling away from the polarimeter.

Implementation Method 1

A light source transmits light from the first optical window to the second optical window

Methodology Applied
Scientific EffectLight transmission: Light

Implementation Method 2

A diffuser viewing screen receives light exiting from the second optical window such that light from the viewing screen can be observed by a user

Methodology Applied
Scientific EffectLight diffusion: Scattering

Data Source

PatentUS9677995B2Sample cell filling device for use remotely from a polarimeter and method of using the same
Publication Date: 2017.06.13 RUDOLPH RESEARCH ANALYTICAL CORP
  • US9677995B2 patent drawing
  • US9677995B2 patent drawing
  • US9677995B2 patent drawing

AI summary

A sample cell filling device for filling a sample cell to be used remotely from a polarimeter is provided. The filling device includes a liquid-sealed housing, light source and a diffuser viewing screen. The housing has a recess for receiving the sample cell, the sample cell having first and second optical windows at the respective ends. A light source transmits light from one optical window to the other optical window. A diffuser viewing screen receives light exiting from the sample cell such that light from the viewing screen can be observed by a user to determine the quality of the sample fill.