Remote Sublimation Apparatus for Radionuclide Purification

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing sublimation apparatuses face challenges in maintaining a vacuum tight seal, particularly when handling large quantities of radioactive materials, which requires complex manipulation within a shielded environment.

Innovation Solution

A remotely controlled sublimation apparatus designed for use in a shielded environment, featuring a crucible block that is movable between open and closed positions, allowing for remote operation of heating elements and vacuum control, thereby simplifying the process of maintaining a seal.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If manual manipulation is used within a shielded environment to maintain a vacuum tight seal, then the seal can be maintained, but the complexity of manipulation and safety risks increase

Engineering Contradiction:
Improvevacuum tight sealVSAvoidmanipulation complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

A remotely controlled manipulator system serves as an intermediary between the operator and the sublimation apparatus. The manipulator can be positioned outside the shielded environment or at a safe distance, allowing the operator to control seal maintenance operations remotely without direct exposure to radioactive materials, thereby reducing manipulation complexity and safety risks while maintaining vacuum integrity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

Manual mechanical manipulation is replaced with a remotely controlled automated system. The remote control mechanism allows operators to perform seal maintenance operations without physically manipulating components within the shielded environment, substituting direct mechanical interaction with remote-controlled actuation, thus simplifying the manipulation process and enhancing safety

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Reliability

If manual manipulation is used within a shielded environment, then seal maintenance is possible, but safety risks and operational difficulty increase

Engineering Contradiction:
Improvevacuum tight sealVSAvoidoperation ease
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The remotely controlled manipulator acts as an intermediary that bridges the gap between the operator and the hazardous environment. Operators can maintain vacuum seals through remote control interfaces located outside the shielded area, eliminating the need for direct manual manipulation within the radioactive environment and significantly improving operational ease and safety

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The system enables self-service operation where the remotely controlled manipulator can autonomously perform seal maintenance tasks based on operator commands. The apparatus can maintain its own vacuum integrity without requiring operators to physically intervene within the shielded environment, making the system easier and safer to operate

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The apparatus enables efficient purification and isolation of radionuclides while ensuring safety by allowing remote operation, reducing the need for manual manipulation within a shielded environment and enhancing the ease and safety of the sublimation process.

Implementation Method 1

selectively heating a solid mixture containing the desired radionuclide(s) in a way that produces a metal vapor

Methodology Applied
Scientific EffectSublimation: Sublimation

Implementation Method 2

the metal vapor, which condenses within and is collected by a collection vessel that is coupled to the sublimation vessel and subject to vacuum pressure

Methodology Applied
Scientific EffectCondensation: Condensation

Data Source

PatentUS12208363B2Remote sublimination apparatus
Publication Date: 2025.01.28 UCHICAGO ARGONNE LLC
  • US12208363B2 patent drawing
  • US12208363B2 patent drawing
  • US12208363B2 patent drawing

AI summary

A remotely controllable sublimation apparatus that includes a crucible block adapted to retain a crucible containing a solid mixture comprising one or more radionuclides, a first heating block comprising one or more first heating elements configured to selectively generate heat having a first temperature sufficient to at least partially sublime the solid mixture, and a collection vessel coupled to the first heating block. The crucible block is movable, relative to the first heating block, between an open position and a closed positon. When the crucible block is in the closed position, the one or more first heating elements are configured to heat the crucible block to the first temperature, thereby heating the solid mixture and producing a vapor that is collected by the collection vessel and leaving a solid residue in the crucible that substantially consists only of the one or more radionuclides.