Surface Fouling Detection via Replica Sensor Monitoring

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Solution Overview

Problem

Current methods for detecting surface fouling, particularly at the nanoscale, are inadequate as they lack real-time, non-invasive monitoring capabilities, leading to inefficient industrial processes due to the inability to accurately detect early-stage fouling before significant performance reduction occurs.

Innovation Solution

A method involving a surface sensitive sensor system with a deposition material that replicates the physico-chemical properties of the industrial surface, capable of detecting foulant accumulation from 1 ng/cm2 to 0.1 mg/cm2, connected to a data acquisition system for real-time monitoring, allowing for early detection and minimally invasive assessment of fouling behavior.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If conventional optical methods (microscopy, laser triangulometry, OCT) are used to monitor surface fouling, then real-time monitoring capability is achieved, but detection sensitivity is insufficient for nanoscale fouling layers

Engineering Contradiction:
Improvedetection sensitivityVSAvoidmeasurement capability
Core Design Contradiction:
Measurement precisionVSDifficulty of detecting and measuring

Solution Approach 1:

The invention creates a replica surface that copies the physico-chemical properties of the industrial surface to be monitored. This replica surface is deposited on a sensor substrate, allowing indirect measurement of fouling behavior with high sensitivity while the original industrial surface continues its operation without interference.

Inventive Principle:
Principle #26Copying

Solution Approach 2:

The replica surface acts as an intermediary between the foulant flow and the sensor substrate. It transfers the fouling information from the industrial surface conditions to the sensor, enabling detection of nanoscale fouling layers through the mediator's interaction with foulants.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Measurement precision

If Electrical Impedance Spectroscopy (EIS) is used for fouling detection, then fouling monitoring capability is achieved, but the membrane must be coated with metal layer which alters surface properties and may occlude pores

Engineering Contradiction:
Improvefouling detection capabilityVSAvoidsurface property alteration
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

Instead of coating the original membrane with metal, the invention creates a replica surface that copies only the necessary physico-chemical fouling properties and deposits it on a sensor substrate. This avoids metal coating on the industrial membrane, preserving its original surface properties and pore structure while still enabling EIS-based fouling detection.

Inventive Principle:
Principle #26Copying

3Ease of operation

If Direct Observation through Membrane (DOTM) is used, then real-time particle deposition observation is achieved, but the surface must be completely transparent which limits industrial applications

Engineering Contradiction:
Improvereal-time observation capabilityVSAvoidapplication range
Core Design Contradiction:
Ease of operationVSAdaptability or versatility

Solution Approach 1:

The invention creates a transparent replica surface that copies the fouling behavior of opaque industrial surfaces. This replica is deposited on a sensor substrate that can be observed microscopically, enabling real-time visualization of fouling processes while the original industrial surface maintains its required opacity for its function.

Inventive Principle:
Principle #26Copying

4Measurement precision

If optical sensors are used for fouling detection, then fouling monitoring is achieved, but calibration with known thickness values is required and sensitivity for initial developing layers is insufficient

Engineering Contradiction:
Improvefouling detection accuracyVSAvoidcalibration requirement
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The replica surface approach allows the sensor to directly measure fouling behavior under actual process conditions without requiring calibration with artificial thickness standards. The replica faithfully reproduces the fouling kinetics and mechanisms, enabling direct interpretation of sensor signals in terms of fouling development stages.

Inventive Principle:
Principle #26Copying

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables accurate, real-time monitoring and prediction of fouling behavior at industrial surfaces, allowing for timely intervention to prevent irreversible performance loss and optimize cleaning procedures, thereby enhancing process efficiency and surface longevity.

Implementation Method 1

providing a sensor system comprising at least one surface sensitive sensor unit, wherein a deposition material is deposited on said surface sensitive sensor unit

Methodology Applied
Scientific EffectSurface-sensitive detection:

Data Source

PatentUS11988595B2Method and device for the detection and monitoring of surface fouling
Publication Date: 2024.05.21 UNIV DEL PAIS VASCO EUSKAL HERRIKO UNIBERTSITATEA
  • US11988595B2 patent drawing
  • US11988595B2 patent drawing
  • US11988595B2 patent drawing

AI summary

A method for the detection and monitoring of surface fouling from the nanoscale as a predictive or real-time monitoring tool is provided. Also provided are devices for carrying out the method, and to uses of the method, in particular for optimising cleaning procedures of devices or components thereof fouled by flows of foulant.