Reservoir Fluid Composition Analysis via Direct Flash Separation

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Solution Overview

Problem

Conventional methods for determining reservoir fluid composition, such as distillation and gas chromatography, face challenges in accurately analyzing heavy fractions and identifying oil-based mud contamination due to limitations in extended gas chromatographic analysis and liquid carryover issues.

Innovation Solution

A direct flash separator system is used to depressurize a single-phase fluid, separating it into gas and liquid phases, and then analyzing the composition using gas chromatography, with recirculation to equilibrate components and determine the atmospheric gas-oil ratio, allowing for accurate calculation of hydrocarbon composition up to C45+ fractions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If conventional distillation and gas chromatographic techniques are used to determine reservoir fluid composition, then the analysis can be performed with standard equipment, but the accuracy is limited for heavy fractions (C20+) and oil-based mud contamination identification

Engineering Contradiction:
Improvecomposition determination accuracyVSAvoidanalysis range limitation
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The reservoir fluid is separated into multiple fractions based on boiling point ranges using a direct flash separator. The system divides the complex mixture into distinct segments (C1-C4, C5-C9, C10-C19, C20-C39, C40+) that can be analyzed separately, allowing accurate determination of heavy fractions that cannot be resolved by conventional single-stage gas chromatography

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

A direct flash separator is introduced as an intermediary device between the reservoir fluid sample and the analysis system. This separator performs preliminary fractionation of the fluid into distinct boiling point ranges, enabling subsequent gas chromatographic analysis to accurately measure heavy fractions (C20+) and identify oil-based mud contamination that would otherwise be indistinguishable in a direct analysis

Inventive Principle:
Principle #24Intermediary (Mediator)

2Adaptability or versatility

If extended gas chromatographic analysis is attempted to reach higher carbon fractions, then the analysis range can be extended, but liquid carryover into the gas phase causes measurement errors

Engineering Contradiction:
Improveanalysis range extensionVSAvoidcomposition measurement accuracy
Core Design Contradiction:
Adaptability or versatilityVSMeasurement precision

Solution Approach 1:

Before gas chromatographic analysis, the reservoir fluid undergoes preliminary fractionation through direct flash separation. This pre-separation step condenses heavy components (C20+) into the liquid phase while allowing lighter components to remain in the gas phase, preventing liquid carryover into the gas chromatograph and ensuring accurate measurement of heavy fractions

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The system utilizes phase transition principles by controlling pressure and temperature to separate the reservoir fluid into gas and liquid phases. The direct flash separator exploits differences in volatility and phase behavior to partition components into appropriate phases, with heavy fractions (C20+) remaining in the liquid phase and lighter fractions vaporizing, thereby enabling accurate analysis of each phase without cross-contamination

Inventive Principle:
Principle #36Phase transitions

3Device complexity

If conventional methods are used to identify oil-based mud contamination, then the process is simpler, but the ability to identify and quantify OBM and generate decontaminated composition is challenging

Engineering Contradiction:
Improveprocess simplicityVSAvoidOBM identification accuracy
Core Design Contradiction:
Device complexityVSMeasurement precision

Solution Approach 1:

The direct flash separator divides the contaminated reservoir fluid into distinct fractions based on boiling point characteristics. Oil-based mud components, which have different volatility profiles than hydrocarbons, are segregated into specific fractions, enabling identification and quantification of OBM contamination and generation of decontaminated composition data

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method provides reliable and repeatable results for higher molecular weight compositions and improved estimation of oil-based mud content, enhancing the accuracy of reservoir fluid analysis and enabling better production planning by extending the determination of reservoir oil composition to C45+ fractions.

Implementation Method 1

depressurizing a single-phase fluid to atmospheric pressure to separate a gas phase from a liquid phase

Methodology Applied
Scientific EffectPhase separation: Phase Change

Implementation Method 2

recirculating a portion of the gas phase through the liquid phase at atmospheric pressure to equilibrate components in the gas phase and components in the liquid phase

Methodology Applied
Scientific EffectEquilibration: Diffusion

Data Source

PatentUS12013387B2Determining reservoir fluid composition to pentatetracontanes plus
Publication Date: 2024.06.18 SAUDI ARABIAN OIL CO
  • US12013387B2 patent drawing
  • US12013387B2 patent drawing
  • US12013387B2 patent drawing

AI summary

Methods and a system for determining a composition of a fluid from a reservoir are provided. An exemplary method includes depressurizing a single-phase fluid to atmospheric pressure to separate a gas phase from a liquid phase, recording the volume of the gas phase, determining the weight of the liquid phase, and determining an atmospheric gas-oil ratio (GOR) from the volume of the gas phase and the weight of the liquid phase. The method also includes determining the composition of the gas phase to C9+, measuring the density of the liquid phase, determining the molecular weight of the liquid phase, and determining the composition of the liquid phase to C45+. The total hydrocarbon composition of the fluid is calculated from the amount of the gas phase, the amount of the liquid phase, the composition of gas phase, the composition liquid phase, and the atmospheric GOR.