Resin-Based LCM Compositions for High-Pressure Well Sealing

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Solution Overview

Problem

Conventional lost circulation materials (LCMs) are ineffective in high-pressure formations and high-injectivity zones, leading to fluid loss during drilling and cementing operations, resulting in increased costs and downtime due to the inability to effectively seal lost circulation zones.

Innovation Solution

The development of LCM compositions comprising a resin, an emulsifier, a crosslinker, a cementitious and/or weighting agent, a retarder, a dispersant, and a silicon-based defoamer, which have a controlled thickening time to form a stable barrier that prevents fluid loss by reaching a Bearden consistency of 100 Bc within 3 to 6 hours, allowing injection through a drill bit to seal lost circulation zones.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional lost circulation materials are used, then the materials can be easily injected, but they are ineffective in high-pressure formations and high-injectivity zones, leading to fluid loss

Engineering Contradiction:
Improvesealing effectivenessVSAvoidfluid loss
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The patent uses a composite material system consisting of resin, emulsifier, crosslinker, and cementitious/weighting agents. This composite formulation creates an LCM composition that can effectively seal lost circulation zones in high-pressure formations while maintaining injectability. The combination of these materials provides both the sealing effectiveness and the rheological properties needed for successful injection and placement.

Inventive Principle:
Principle #40Composite materials

2Productivity

If the LCM composition thickens too quickly, then it forms a seal faster, but it becomes difficult to inject through the drill bit

Engineering Contradiction:
Improvesealing speedVSAvoidinjectability
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The patent controls the thickening behavior by adjusting formulation parameters including the type and amount of resin, emulsifier concentration, crosslinker dosage, and water-to-cement ratio. These parameter changes allow the LCM composition to maintain proper rheology for injection through the drill bit while still achieving adequate thickening and sealing within the required time frame. The retarder component specifically manages the thickening rate to balance injectability with sealing speed.

Inventive Principle:
Principle #35Parameter changes

3Stress or pressure

If the LCM composition is too dense, then it provides better weighting and sealing pressure, but it requires more energy to inject and may not reach the lost circulation zone effectively

Engineering Contradiction:
Improvesealing pressureVSAvoidinjection energy
Core Design Contradiction:
Stress or pressureVSUse of energy by moving object

Solution Approach 1:

The patent incorporates weighting agents at controlled concentrations (typically 5-20% by weight of cement) to provide localized density enhancement where needed for sealing pressure, while maintaining overall composition density that allows effective injection. This local quality approach ensures sufficient sealing pressure at the lost circulation zone without requiring excessive injection energy throughout the entire fluid column.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The LCM compositions provide a stable and effective seal in high-pressure formations and high-injectivity zones, reducing fluid loss and maintaining stability, thus reducing operational costs and downtime by forming a durable barrier that prevents fluid penetration into the formation.

Implementation Method 1

LCM compositions may include a resin; an emulsifier selected from the group consisting of ethoxylated phenol, sodium salt of modified tall oil fatty amide, carboxylic acid terminated fatty polyamide, modified amidoamine, tall oil fatty acid, oxidized tall oil fatty amidoamine, ether carboxylic acid, and combinations thereof

Methodology Applied
Scientific EffectEmulsion: Emulsion

Implementation Method 2

The LCM compositions may have a thickening time of from about 3 hours than about 6 hours by reaching a Bearden consistency of 100 Bc

Methodology Applied
Scientific EffectThickening: Rheopecty

Implementation Method 3

a crosslinker

Methodology Applied
Scientific EffectCrosslinking: Chemical Bonding

Implementation Method 4

a cementitious and/or weighting agent

Methodology Applied
Scientific EffectSedimentation: Sedimentation

Implementation Method 5

a dispersant

Methodology Applied
Scientific EffectDispersion: Dispersion (of waves)

Implementation Method 6

a silicon-based defoamer

Methodology Applied
Scientific EffectDefoaming: Antifoam

Data Source

PatentUS11905458B2Loss circulation materials for high pressure formations
Publication Date: 2024.02.20 SAUDI ARABIAN OIL CO
  • US11905458B2 patent drawing
  • US11905458B2 patent drawing
  • US11905458B2 patent drawing

AI summary

Lost circulation material (LCM) compositions may include a resin; an emulsifier selected from the group consisting of ethoxylated phenol, sodium salt of modified tall oil fatty amide, carboxylic acid terminated fatty polyamide, modified amidoamine, tall oil fatty acid, oxidized tall oil fatty amidoamine, ether carboxylic acid, and combinations thereof; a crosslinker, a cementitious and/or weighting agent; a retarder; a dispersant; and a silicon-based defoamer. The LCM compositions may have a thickening time of from about 3 hours than about 6 hours by reaching a Bearden consistency of 100 Bc. Methods of eliminating or reducing lost circulation in a lost circulation zone from a well may include introducing these LCM compositions into the well.