Resin Particle Silica Surface Modification for Toner Fluidity

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Resin particles used in toners, powder coating materials, and slush molding lack effective methods to enhance strength and fluidity while preventing silica particle embedding and detachment, due to limitations in silica particle shape and distribution.

Innovation Solution

The development of resin particles with silica particles externally added to the surface, having a specific size distribution and circularity, which maintains heterogeneous shape and fluidity under mechanical load, achieved by controlling the volume average particle diameter, particle size distribution index, and average circularity of the silica particles.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If silica particles are added to enhance strength and fluidity, then the resin particle strength and fluidity are improved, but the silica particles may embed into or detach from the resin particle surface

Engineering Contradiction:
Improveresin particle strengthVSAvoidsilica particle attachment stability
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The patent applies parameter changes by precisely controlling the volume average particle diameter (100-500 nm), particle size distribution index (1.40-1.80), and average circularity (0.5-0.85) of silica particles. These parameter optimizations ensure that silica particles maintain stable attachment to the resin particle surface while enhancing strength and fluidity, preventing both embedding and detachment.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite structure by combining resin particles with specifically designed silica particles. The silica particles with controlled heterogeneous shapes and size distributions form a stable composite system where the silica particles are externally added onto the resin mother particle surface, achieving both strength enhancement and attachment stability.

Inventive Principle:
Principle #40Composite materials

2Adaptability or versatility

If silica particles with various shapes are used to functionalize resin particles, then the resin particle functionality is enhanced, but the manufacturing precision and control of silica particle distribution become difficult

Engineering Contradiction:
Improveresin particle functionalityVSAvoidsilica particle distribution control
Core Design Contradiction:
Adaptability or versatilityVSManufacturing precision

Solution Approach 1:

The patent establishes precise parameter ranges including volume average particle diameter (100-500 nm), particle size distribution index (1.40-1.80), and average circularity (0.5-0.85). These parameter specifications enable controlled manufacturing of silica particles with heterogeneous shapes while maintaining precise distribution and attachment characteristics on the resin particle surface.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies local quality by creating silica particles with heterogeneous shapes (circularity 0.5-0.85) that are specifically designed for their local function of enhancing resin particle fluidity and strength. The non-spherical shapes provide localized surface area variations that improve attachment stability without compromising manufacturing precision.

Inventive Principle:
Principle #3Local quality

3Ease of operation

If silica particles with small size are used to prevent packing, then the resin particle fluidity is improved, but the silica particles may embed into the resin particle more easily

Engineering Contradiction:
Improveresin particle fluidityVSAvoidsilica particle embedding
Core Design Contradiction:
Ease of operationVSObject-affected harmful factors

Solution Approach 1:

The patent optimizes the volume average particle diameter of silica particles to the specific range of 100-500 nm. This parameter control ensures that silica particles are small enough to maintain resin particle fluidity and prevent packing, while simultaneously large enough to resist embedding into the resin particle surface when properly attached.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a stable composite structure where silica particles with controlled dimensions (100-500 nm) are externally added onto the resin mother particle. This composite approach ensures that the silica particles maintain sufficient size to prevent embedding while being small enough to enhance fluidity, achieving both goals simultaneously.

Inventive Principle:
Principle #40Composite materials

Data Source

PatentUS9394413B2Resin particle and method for producing the same
Publication Date: 2016.07.19 FUJIFILM BUSINESS INNOVATION CORP

AI summary

A resin particle having: a resin mother particle; and silica particles external added onto the surface of the resin mother particle, wherein a primary particles of the silica particles which have a volume average particle diameter of from 100 nm to 500 nm, a particle size distribution index of from 1.40 to 1.80 and an average circularity of from 0.5 to 0.85 has a regression line expressed by the following expression (1) with respect to the circularity and the volume average particle diameter (nm):Circularity=α×(Volume average particle diameter)/1000+β  (1)wherein α is from −2.5 to −0.9, and β is from 0.8 to 1.2.