Resistant Dextrin Production via Mild Vacuum Condensation

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Solution Overview

Problem

Existing methods for producing polydextrose as a low-calorie bulking agent face challenges such as harsh production conditions, undesirable color and flavor, and low molecular weight, with previous solutions either being complex or costly, and the use of polyols which are increasingly objectionable to consumers.

Innovation Solution

A method involving the reaction of starch hydrolyzates and dextrose under mild vacuum conditions without external plasticizers, using citric acid as a catalyst, to produce digestion-resistant dextrins with higher molecular weight and improved properties, potentially replacing polydextrose in food applications.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If polydextrose is produced by condensation reaction under harsh conditions, then low-calorie bulking agent is obtained, but the product has dark color and undesirable acidic and bitter flavor

Engineering Contradiction:
Improvecaloric value reductionVSAvoidcolor and flavor quality
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The patent changes the reaction parameters from harsh conditions to milder conditions, specifically conducting the condensation reaction at lower temperatures (below 100°C) and shorter reaction times, which prevents excessive browning and flavor degradation while still achieving polydextrose formation

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses enzyme (amyloglucosidase) as an intermediary catalyst to facilitate the condensation reaction under milder conditions, replacing traditional harsh chemical catalysts and enabling controlled polymerization without excessive heat or acid that cause dark color and bitter flavor

Inventive Principle:
Principle #24Intermediary (Mediator)

2Quantity of substance

If polydextrose is produced to achieve low caloric value, then bulking agent function is obtained, but molecular weight is low and product quality is compromised

Engineering Contradiction:
Improvecaloric valueVSAvoidmolecular weight control
Core Design Contradiction:
Quantity of substanceVSManufacturing precision

Solution Approach 1:

The patent employs continuous enzymatic hydrolysis followed by controlled evaporation and concentration to progressively build up the polymer chains, allowing sustained molecular weight increase without interrupting the reaction process, resulting in higher quality polydextrose with appropriate molecular weight

Inventive Principle:
Principle #20Continuity of useful action

3Quantity of substance

If traditional polydextrose production methods are used, then low-calorie bulking agent is produced, but processing complexity and cost increase

Engineering Contradiction:
Improvecaloric value reductionVSAvoidprocessing steps
Core Design Contradiction:
Quantity of substanceVSDevice complexity

Solution Approach 1:

The patent combines multiple processing steps into a simplified sequence: enzymatic hydrolysis of starch to glucose, followed by controlled evaporation and concentration to achieve polydextrose formation in situ, eliminating the need for separate purification, drying, and granulation steps required by traditional methods

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method produces dextrins with improved texture and taste, higher molecular weight, and reduced processing complexities and costs, eliminating the need for polyols and harsh acids, resulting in a more consumer-friendly and cost-effective low-calorie bulking agent.

Implementation Method 1

A method involving the reaction of starch hydrolyzates and dextrose under mild vacuum conditions without external plasticizers, using citric acid as a catalyst, to produce digestion-resistant dextrins with higher molecular weight

Methodology Applied
Scientific EffectCondensation reaction:

Implementation Method 2

using citric acid as a catalyst, to produce digestion-resistant dextrins

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

reaction of starch hydrolyzates and dextrose under mild vacuum conditions

Methodology Applied
Scientific EffectVacuum evaporation: Vacuum Distillation

Data Source

PatentUS9422372B2Production of resistant dextrins
Publication Date: 2016.08.23 GRAIN PROCESSING CORP
  • US9422372B2 patent drawing

AI summary

A method for producing digestion-resistant dextrin from starch hydrolyzates is disclosed. In one form, the method includes mixing the starch hydrolyzate, dextrose and an acid catalyst which are allowed to react under mild vacuum with heat. The ingredients require no pre-drying and the method requires no external plasticizers.