Stabilizing Retained Austenite in Reference Pieces via Nano-Crystallization

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Solution Overview

Problem

Existing methods for manufacturing reference pieces to measure retained austenite are prone to measurement variations due to the potential transformation of austenite into martensite from impact or time lapse, affecting hardness and product dimensions.

Innovation Solution

A manufacturing method involving nano-crystallization of a metal member's surface followed by quenching and tempering to stabilize retained austenite, ensuring a uniform diffraction profile and minimizing measurement deviations.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If a reference piece is prepared for measuring retained austenite, then measurement of retained austenite can be performed, but the retained austenite may transform into martensite due to impact or time lapse causing measurement variations

Engineering Contradiction:
Improvemeasurement precision of retained austeniteVSAvoidstability of retained austenite
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The patent applies preliminary action by performing nano-crystallization on the metal member's surface before quenching and tempering. This pre-treatment creates a refined grain structure that stabilizes the retained austenite, preventing its transformation into martensite during subsequent storage or measurement processes, thereby ensuring measurement reliability

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent employs parameter changes by controlling the quenching and tempering conditions after nano-crystallization. By optimizing the heating temperature, holding time, and cooling rate during heat treatment, the patent achieves a stable microstructure with controlled retained austenite content that resists temporal changes and impact-induced transformation

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If quenching is performed to obtain retained austenite, then austenite remains in the metal, but the retained austenite is unstable and transforms into martensite over time

Engineering Contradiction:
Improveamount of retained austeniteVSAvoidstability of austenite structure
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

Nano-crystallization is performed as a preliminary treatment before quenching to create a refined grain structure. This pre-treatment stabilizes the austenite phase by reducing grain size and increasing grain boundary density, which prevents the retained austenite from transforming into martensite during subsequent storage

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent creates a composite microstructure consisting of nanocrystalline regions with retained austenite and tempered martensite. This composite structure, achieved through the combination of nano-crystallization and heat treatment, provides both the desired amount of retained austenite and enhanced stability against transformation

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces a stable reference piece with reduced measurement variations, maintaining a consistent austenite ratio and resisting temporal changes, thus enhancing the accuracy of retained austenite measurement.

Implementation Method 1

performing nano-crystallization on at least a portion of a surface of the metal member

Methodology Applied
Scientific EffectNano-crystallization: Crystallisation

Implementation Method 2

performing quenching and tempering a metal member after performing nano-crystallization

Methodology Applied
Scientific EffectAustenitization: Heating

Implementation Method 3

when the steel is quenched, that is, when the steel is rapidly cooled after the temperature of the γ region is maintained

Methodology Applied
Scientific EffectQuenching: Cooling

Implementation Method 4

performing quenching and tempering a metal member

Methodology Applied
Scientific EffectTempering: Heat Treatment

Data Source

PatentUS20240182994A1Method for manufacturing reference piece for measuring retained austenite
Publication Date: 2024.06.06 SINTOKOGIO LTD
  • US20240182994A1 patent drawing
  • US20240182994A1 patent drawing
  • US20240182994A1 patent drawing

AI summary

The manufacturing method of the reference piece for measuring retained austenite includes performing quenching and tempering a metal member after performing nano-crystallization on at least a portion of a surface of the metal member.