Dielectric Property Measurement Using RF Capacitance Calibration

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Solution Overview

Problem

Current methods for measuring dielectric properties of parts in plasma processing systems are inaccurate due to the use of small sample coupons that may not represent the material composition of full-sized parts, and the measurements are often taken at different frequencies than those used in plasma processing, leading to extrapolation errors.

Innovation Solution

A method involving an apparatus with an electrically grounded chamber, a lower electrode connected to an RF transmission rod, and an upper electrode, which uses a capacitance meter to measure capacitance between the RF rod and the upper electrode at various separation distances, allowing for the determination of dielectric constant and loss tangent by simulating the resonance frequency and calculating the capacitance of the part.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of time

If small sample coupons are used for measurement, then measurement time and complexity are reduced, but measurement precision deteriorates because the sample may not represent the material composition of the full-sized part

Engineering Contradiction:
Improvemeasurement timeVSAvoiddielectric property accuracy
Core Design Contradiction:
Loss of timeVSMeasurement precision

Solution Approach 1:

The measurement process is segmented into two distinct phases: (1) calibration phase using small sample coupons to establish the relationship between capacitance and dielectric properties, and (2) measurement phase using the calibrated apparatus with the full-sized part. This segmentation allows the benefits of quick small-sample calibration while achieving accurate full-part measurement results.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The small sample coupon serves as a representative copy or model of the full-sized part's material composition. By calibrating the measurement system with the coupon (copy) and then applying the same measurement parameters to the actual part, the system transfers the calibration data to achieve accurate measurements without requiring the coupon itself to be the full-sized part.

Inventive Principle:
Principle #26Copying

2Adaptability or versatility

If dielectric properties are measured at different frequencies than operating frequency, then measurement flexibility is improved, but measurement precision deteriorates due to frequency-dependent dielectric properties requiring extrapolation

Engineering Contradiction:
Improvemeasurement frequency flexibilityVSAvoiddielectric property accuracy at operating frequency
Core Design Contradiction:
Adaptability or versatilityVSMeasurement precision

Solution Approach 1:

The system performs preliminary calibration measurements at the actual operating frequency (e.g., 13.56 MHz) before conducting the actual dielectric property measurement. By pre-establishing the capacitance-dielectric property relationship at the correct frequency through calibration, the system eliminates the need for frequency extrapolation and ensures measurement accuracy at the operating frequency.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The measurement system dynamically adjusts the RF frequency parameter to match the actual operating frequency of the plasma processing equipment. By changing the frequency parameter from a fixed calibration frequency to the variable operating frequency, the system ensures that dielectric properties are measured at the correct frequency without requiring extrapolation.

Inventive Principle:
Principle #35Parameter changes

3Measurement precision

If full-sized parts are measured directly, then measurement precision is improved, but device complexity and measurement time increase

Engineering Contradiction:
Improvedielectric property accuracyVSAvoidmeasurement apparatus complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The small sample coupon acts as an intermediary element in the measurement process. It is used to calibrate the measurement system and establish the capacitance-dielectric property relationship, serving as a mediator between the measurement apparatus and the full-sized part. This intermediary approach simplifies the overall process by separating calibration from measurement.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The measurement process is divided into calibration (using coupon) and measurement (using full part) segments. This segmentation reduces device complexity by allowing the use of a simpler calibration setup with the coupon, while the full measurement apparatus only needs to perform the actual measurement at operating frequency without requiring complex calibration mechanisms.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables accurate measurement of dielectric properties of full-sized parts at the operating frequency of RF power, reducing extrapolation errors and providing precise data for plasma processing systems.

Implementation Method 1

using the capacitance meter to measure and record the capacitance between the RF rod and the upper electrode

Methodology Applied
Scientific EffectCapacitance: Capacitance

Implementation Method 2

transmitting radiofrequency (RF) power through a processing gas

Methodology Applied
Scientific EffectElectromagnetic induction: Electromagnetic Induction

Implementation Method 3

a plasma is generated by transmitting radiofrequency (RF) power through a processing gas

Methodology Applied
Scientific EffectDielectric heating: Dielectric Heating

Data Source

PatentUS7973539B1Methods for measuring dielectric properties of parts
Publication Date: 2011.07.05 LAM RES CORP
  • US7973539B1 patent drawing
  • US7973539B1 patent drawing
  • US7973539B1 patent drawing

AI summary

A method is disclosed for calibrating a capacitance of an apparatus for measuring dielectric properties of a part. The apparatus includes an electrically grounded chamber, a lower electrode disposed within the chamber and connected to a radiofrequency (RF) transmission rod, an electrically grounded upper electrode disposed within the chamber above the lower electrode, and a variable capacitor connected to control transmission of RF power through the RF transmission rod to the lower electrode. A method is also disclosed for determining a capacitance of a part through use of the apparatus. A method is also disclosed for determining a dielectric constant of a part through use of the apparatus. A method is also disclosed for determining a loss tangent of a part through use of the apparatus.