Deagglomerating Superabsorbent Polymer Agglomerates via Roll Compression

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Solution Overview

Problem

The production of superabsorbent polymer particles often results in agglomerates during surface postcrosslinking, which are difficult to deagglomerate without compromising product quality, and existing methods either mill or cut the particles, damaging the outer shell and limiting effective deagglomeration.

Innovation Solution

A process involving the use of a roll crusher with specific surface roughness and gap width to deagglomerate the oversize fraction of surface postcrosslinked superabsorbent polymer particles, allowing for moderate mechanical stress that breaks agglomerates without damaging primary particles, and recycling these particles before or into classification.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If existing deagglomeration methods (milling or cutting) are used to break agglomerates, then deagglomeration is achieved, but the outer shell is damaged and product quality is compromised

Engineering Contradiction:
Improveouter shell integrityVSAvoiddeagglomeration effectiveness
Core Design Contradiction:
Stability of the object's compositionVSProductivity

Solution Approach 1:

The invention changes the mechanical parameters of the deagglomeration process by using a roll crusher with specific gap width (0.5-2.0 mm) and roll surface characteristics, transforming the action from intensive milling/cutting to moderate compression that breaks agglomerates while preserving the outer shell

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces the traditional milling or cutting mechanical systems with a roll crusher system that uses controlled compression between two rolls, substituting the harmful mechanical action with a gentler compression-based deagglomeration mechanism

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Ease of manufacture

If moderate mechanical stress is applied to deagglomerate particles, then agglomerates are broken without damaging primary particles, but the process requires specific equipment configuration

Engineering Contradiction:
Improvedeagglomeration process simplicityVSAvoidroll crusher configuration requirements
Core Design Contradiction:
Ease of manufactureVSDevice complexity

Solution Approach 1:

The invention establishes specific parameter ranges for the roll crusher (gap width 0.5-2.0 mm, roll surface roughness Rz 0.01-25 μm) that optimize the balance between deagglomeration effectiveness and outer shell preservation, making the process economically viable despite equipment requirements

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method effectively deagglomerates agglomerates without impacting product quality, maintaining the high crosslinking density of the outer shell and improving the overall quality of the superabsorbent polymer particles by avoiding attrition and cutting, thus enhancing their properties.

Implementation Method 1

the superabsorbent polymer particles of the oversize fraction are deagglomerated using a roll crusher... Preferably, the teeth of the double toothed roll crusher have rounded edges so that the roll crusher deagglomerates the agglomerates mainly by compression

Methodology Applied
Scientific EffectCompression: Compression

Data Source

PatentUS11680142B2Process for producing superabsorbent polymer particles
Publication Date: 2023.06.20 BASF SE

AI summary

The invention relates to a process for producing superabsorbent polymer particles, comprising surface postcrosslinking, classifying the surface postcrosslinked superabsorbent polymer particles, deagglomerating the separated oversize fraction using a roll crusher and recycling the disintegrated oversize fraction before or into the classification of the surface postcrosslinked superabsorbent polymer particles.