Room Temperature Silicone Adhesion via Peroxide Catalyst and Vacuum

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Solution Overview

Problem

Conventional silicone adhesives require high temperature and pressure for curing, necessitating the use of platinum-containing primers and furnaces or autoclaves, which can be inefficient and damage other materials like epoxy or urethane components.

Innovation Solution

A method using a platinum catalyzed silane primer with a fugitive inhibitor and a room temperature-stable silicone film adhesive catalyst, applied under vacuum and pressure to adhere structures without the need for additional heat, allowing for efficient bonding at room temperature.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If platinum-containing primers and high temperature pressure curing are used, then adhesion strength is improved, but device complexity and energy consumption increase

Engineering Contradiction:
Improveadhesion strengthVSAvoidcuring system complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent changes the curing parameters from high temperature (300-350°F) and high pressure to room temperature and atmospheric pressure by using a peroxide catalyst instead of platinum catalyst, eliminating the need for specialized furnaces or autoclaves while maintaining adhesion strength

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses a disposable peroxide catalyst that provides sufficient catalytic activity at room temperature without requiring expensive platinum catalysts and complex curing equipment, reducing both material cost and device complexity

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Reliability

If high temperature curing is used, then adhesive curing is achieved, but sensitive materials are damaged

Engineering Contradiction:
Improveadhesive curingVSAvoidheat damage to sensitive materials
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent changes the curing temperature parameter from high temperature (300-350°F) to room temperature by switching to a peroxide catalyst system, achieving complete adhesive curing without exposing sensitive materials like epoxy or urethane to damaging heat

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The peroxide catalyst acts as an intermediary that enables the silicone adhesive to cure at room temperature through a different chemical mechanism, avoiding the need for high temperature while still achieving reliable bond formation

Inventive Principle:
Principle #24Intermediary (Mediator)

3Strength

If platinum catalyzed silane primer is used, then adhesion is improved, but catalyst stability at room temperature deteriorates

Engineering Contradiction:
ImproveadhesionVSAvoidcatalyst stability
Core Design Contradiction:
StrengthVSStability of the object's composition

Solution Approach 1:

The patent uses a peroxide catalyst that is stable at room temperature and does not require the expensive platinum catalyst, providing sufficient catalytic activity for curing without the stability issues associated with platinum-based systems

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The patent changes the catalyst type from platinum to peroxide, which fundamentally alters the stability characteristics to allow room temperature storage and handling while maintaining curing capability

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables efficient adhesion of structures using a silicone adhesive system at room temperature, eliminating the need for high-temperature curing and protecting sensitive materials from excessive heat.

Implementation Method 1

the catalyst may be selected from a group consisting of peroxide and platinum

Methodology Applied
Scientific EffectPeroxide catalysis: Catalysis

Implementation Method 2

a platinum catalyzed silane primer specially formulated for use with platinum catalyzed or peroxide catalyzed adhesive systems

Methodology Applied
Scientific EffectSilane polymerization: Chemical Bonding

Implementation Method 3

The period of time includes a sufficient time to remove the primer fugitive inhibitor so as to permit the first and second pre-adhered surfaces to be adhered to one another through the curing of the film adhesive

Methodology Applied
Scientific EffectVacuum: Vacuum

Data Source

PatentUS10106712B2Method for adhering structures using silicone adhesive system
Publication Date: 2018.10.23 RTX CORP
  • US10106712B2 patent drawing
  • US10106712B2 patent drawing

AI summary

A method of adhering a first structure to a second structure using a primer, containing a primer fugitive inhibitor, and a film adhesive by removing the primer fugitive inhibitor under vacuum at room temperature conditions.