Rotating Electrode Corrosion Testing Device

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Solution Overview

Problem

Current methods for evaluating corrosion inhibitors in circulating cooling water systems fail to accurately simulate the hydraulic conditions of the system, leading to inaccurate results and human error, particularly due to the inability to simultaneously test corrosion from both liquid and condensed gas, and the complexity of electrochemical methods.

Innovation Solution

A device comprising a five-port glass tube and a three-electrode system that simulates the hydraulic conditions of a circulating cooling water system, allowing for dynamic testing of corrosion inhibitors by controlling flow velocity and temperature, and using AC impedance spectroscopy to evaluate corrosion inhibition performance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If conventional electrochemical methods are used with a three-electrode system in a static state, then the testing can be performed in the laboratory, but the electrode surface cannot simulate the hydraulic condition of the circulating cooling water system, leading to concentration polarization and inaccurate results

Engineering Contradiction:
Improveaccuracy of corrosion testing resultVSAvoidability to simulate hydraulic condition
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent transforms the static three-electrode system into a dynamic testing setup where the working electrode rotates within the circulating cooling water flow. This rotation enables the electrode surface to experience hydraulic conditions similar to actual pipe surfaces, eliminating concentration polarization and improving measurement accuracy while maintaining laboratory testing capabilities

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent creates a simplified model system that copies the essential hydraulic conditions of the circulating cooling water system. By using a rotating electrode that mimics the flow conditions over pipe surfaces, the system reproduces real-world corrosion environments in the laboratory without requiring actual pipeline installation

Inventive Principle:
Principle #26Copying

2Measurement precision

If AC impedance spectroscopy method is used, then the testing can be performed, but the high requirement on the relative position of the electrodes causes difficulty for installation on the circulating cooling water system

Engineering Contradiction:
Improvetesting capabilityVSAvoidinstallation difficulty
Core Design Contradiction:
Measurement precisionVSEase of operation

Solution Approach 1:

The patent divides the testing system into separate functional components: a rotating working electrode assembly, a stationary reference electrode, and an auxiliary electrode. This segmentation allows each electrode to be positioned independently according to its specific requirements, simplifying installation while maintaining the precise relative positioning needed for accurate AC impedance spectroscopy measurements

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

By making the working electrode rotatable rather than fixed, the system provides flexibility in installation. The electrode can be positioned at the correct radial distance from the center and rotated to achieve proper orientation, making the system easier to install on circulating cooling water systems while maintaining the geometric requirements for accurate measurements

Inventive Principle:
Principle #15Dynamics

3Measurement precision

If rotary coupon method is used, then the corrosion condition can be directly reflected close to actual working condition, but treatments of the test piece before and after corrosion are necessary, causing errors due to human factors and requiring time-consuming operations

Engineering Contradiction:
Improvereflection of actual corrosion conditionVSAvoidtesting efficiency
Core Design Contradiction:
Measurement precisionVSProductivity

Solution Approach 1:

The rotating electrode system automatically maintains itself during testing through continuous rotation, which prevents scale buildup and ensures uniform exposure to the corrosive environment. This self-cleaning action eliminates the need for manual treatment of test pieces before and after testing, removing sources of human error and significantly improving testing efficiency while maintaining accurate reflection of corrosion conditions

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The continuous rotation of the working electrode ensures uninterrupted exposure to the corrosive medium and continuous data collection. This eliminates the idle time associated with removing, treating, and replacing test pieces in the rotary coupon method, enabling continuous testing and dramatically improving productivity while maintaining the accuracy of corrosion condition assessment

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The device provides accurate and efficient evaluation of corrosion inhibition performance by simulating real-world conditions, reducing human error and enabling fast assessment of corrosion inhibitors under dynamic water conditions.

Implementation Method 1

using AC impedance spectroscopy to evaluate corrosion inhibition performance

Methodology Applied
Scientific EffectAC impedance spectroscopy:

Implementation Method 2

simulating the hydraulic condition of the circulating cooling water by controlling a flow velocity and a temperature

Methodology Applied
Scientific EffectHydraulic flow:

Data Source

PatentUS9182332B2Device and method for testing corrosion inhibitor
Publication Date: 2015.11.10 NANJING UNIV
  • US9182332B2 patent drawing
  • US9182332B2 patent drawing
  • US9182332B2 patent drawing

AI summary

A device for testing a corrosion inhibitor, the device including: a circulating cooling water tank; a circulating water pump; a flowmeter; a five-port glass tube; a working electrode; a reference electrode; an auxiliary electrode; a heating rod; and an electrochemical workstation. The circulating water pump is connected to the circulating cooling water tank. The heating rod is fixed inside the circulating cooling water tank. The water inlet of the flowmeter is connected to the circulating water pump. The water outlet of the flowmeter is connected to the water inlet of the five-port glass tube. The water outlet of the five-port glass tube is connected to the circulating cooling water tank. The working electrode the reference electrode, and the auxiliary electrode are connected to the electrochemical workstation; and the electrochemical workstation is connected to a host computer.