Rotating Membrane Emulsification for Droplet Size Control

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Solution Overview

Problem

Existing membrane emulsification techniques face challenges in producing uniformly sized droplets due to continuous shear forces, which can be difficult to control and optimize for precise droplet formation.

Innovation Solution

A rotating membrane device with a cylindrical porous surface and a vane assembly that applies discontinuous or cyclic shear forces to the dispersible liquid phase, allowing for precise control of droplet size by optimizing the relative speed and spacing of the vanes and membrane, resulting in droplets of 1 to 500 μm in size.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If continuous shear forces are applied to the dispersible liquid phase, then droplets can be formed, but the droplet size uniformity and controllability deteriorate

Engineering Contradiction:
Improvedroplet size uniformityVSAvoidshear force control complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent applies periodic action by using an oscillating membrane that moves back and forth to create cyclic shear forces on the dispersible liquid phase. This periodic motion generates more uniform droplet sizes compared to continuous shear, as the oscillating motion creates consistent shear cycles that control droplet formation. The membrane oscillation can be achieved through mechanical vibration or acoustic waves, providing controllable periodic action.

Inventive Principle:
Principle #19Periodic action

Solution Approach 2:

The patent implements dynamics by using a rotating cylindrical membrane device where the membrane surface rotates relative to the dispersible liquid phase. This dynamic motion creates varying shear forces as different portions of the membrane surface interact with the liquid, improving droplet size uniformity. The rotation speed and direction can be adjusted to optimize droplet formation, making the system adaptable and controllable.

Inventive Principle:
Principle #15Dynamics

2Manufacturing precision

If traditional membrane emulsification techniques are used, then the process is simple, but droplet size control precision deteriorates

Engineering Contradiction:
Improvedroplet size control precisionVSAvoidmembrane device complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent employs a dynamic membrane system that rotates or oscillates to create controlled shear forces during emulsification. This dynamic motion allows precise control over droplet size by adjusting rotation speed or oscillation frequency, while maintaining a relatively simple cylindrical membrane structure. The dynamic element adds control precision without significantly increasing overall device complexity.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent uses periodic membrane oscillation or rotation to create cyclic shear forces that improve droplet size control. The periodic motion creates consistent shear cycles that lead to more uniform droplet formation compared to static membranes. This approach achieves better precision while keeping the device structure simple, as the periodic action is generated by straightforward mechanical or acoustic means.

Inventive Principle:
Principle #19Periodic action

3Ease of operation

If continuous shear forces are applied, then droplet formation occurs, but the ease of optimization deteriorates

Engineering Contradiction:
Improveoptimization easeVSAvoidparameter control complexity
Core Design Contradiction:
Ease of operationVSDevice complexity

Solution Approach 1:

The patent uses a dynamic rotating or oscillating membrane system where operation parameters such as rotation speed or oscillation frequency can be easily adjusted to optimize droplet size. This dynamic control mechanism provides intuitive and straightforward optimization, as operators can simply change the speed or frequency settings without complex adjustments. The single primary control parameter (rotation/oscillation speed) simplifies the optimization process.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent enables easy optimization by allowing straightforward changes in key operating parameters such as membrane rotation speed, oscillation frequency, or amplitude. These parameter changes directly affect droplet size and distribution, providing a simple optimization pathway. The system responds predictably to parameter adjustments, making it easy to achieve desired droplet characteristics without complex multi-parameter optimization.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces more uniform and controllable droplets compared to traditional continuous shear techniques, enabling precise control over droplet formation and size, enhancing the efficiency of emulsion production.

Implementation Method 1

the vanes comprise a shear surface located within 1 mm of the porous surface... the shear surfaces exert shear forces upon the dispersible liquid phase passing through the porous surface to form droplets

Methodology Applied
Scientific EffectShear force: Shear Stress

Data Source

PatentUS9393532B2Swept membrane emulsification
Publication Date: 2016.07.19 ROHM & HAAS CO
  • US9393532B2 patent drawing
  • US9393532B2 patent drawing
  • US9393532B2 patent drawing

AI summary

A method for making an emulsion using a rotating membrane device (10) including:i) a membrane assembly (12) including a cylindrical porous surface (14) enclosing an inner chamber (16) concentrically positioned about an axis (X),ii) a vane assembly (18) including a plurality of vanes (20) extending along the axial length (L) of the porous surface (14) of the membrane assembly (12), wherein the vanes (24) comprise a shear surface (24) located within 1 mm of the porous surface (14), andiii) a vessel (22) enclosing the membrane and vane assemblies (12, 18);wherein the method includes the step of moving a dispersible liquid phase (26) through the porous surface (14) into a continuous liquid phase (28) while rotating at least one of the vane assembly (18) or membrane assembly (12) relative to the other about the axis (X) such that the shear surfaces (24) exert shear forces upon the dispersible liquid phase (26) passing through the porous surface (14) to form droplets (30) of a dispersed liquid phase having a size of 1 to 500 μm within the continuous liquid phase (28).