R-T-B Permanent Magnet Grain Boundary Control

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Solution Overview

Problem

R-T-B based sintered magnets have insufficient residual magnetic flux density and temperature properties, with complex manufacturing processes leading to low productivity.

Innovation Solution

An R-T-B based permanent magnet comprising R2T14B main phase crystal grains with a coverage ratio of 50.0% or more and an area proportion of 92.0% or more, along with a grain boundary structure, which includes controlling the content of C and O to prevent phase formation that degrades coercivity and magnetic properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional R-T-B based sintered magnet manufacturing methods are used, then the manufacturing process can be completed, but the residual magnetic flux density is not sufficiently high

Engineering Contradiction:
Improveresidual magnetic flux densityVSAvoidmanufacturing efficiency
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The patent applies parameter changes by precisely controlling the content of rare-earth elements (27.5-31.5 mass%) and creating a specific microstructure with R2T14B main phase crystal grains having 50.0% or more coverage ratio and 92.0% or more area proportion. This optimized composition and microstructure achieve high residual magnetic flux density (14.0 kG or more) while maintaining manufacturing feasibility

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite material principles by creating a multi-phase structure consisting of R2T14B main phase crystal grains and grain boundaries with controlled impurity distribution. The composite structure of main phase grains (providing magnetic properties) and grain boundaries (controlling coercivity) achieves both high residual magnetic flux density and good temperature properties

Inventive Principle:
Principle #40Composite materials

2Reliability

If conventional sintered rare-earth magnet manufacturing methods are used, then the magnet can be manufactured, but the temperature properties are not sufficient

Engineering Contradiction:
Improvetemperature propertiesVSAvoidmanufacturing process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent applies local quality by creating distinct regions with different functions: R2T14B main phase crystal grains (50.0% or more coverage ratio) providing high magnetic properties at room temperature, and grain boundaries with controlled impurity content (C: 500 ppm or less, O: less than 900 ppm) providing thermal stability. This spatial differentiation of material properties achieves excellent temperature characteristics while using a relatively simple sintering process

Inventive Principle:
Principle #3Local quality

3Productivity

If conventional R-T-B based sintered magnet methods are used, then manufacturing can proceed, but productivity is low due to complicated manufacturing steps

Engineering Contradiction:
Improvemanufacturing productivityVSAvoidmanufacturing process complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent merges multiple process steps into a simplified sintering process that simultaneously achieves: (1) formation of R2T14B main phase crystal grains with 50.0% or more coverage ratio, (2) creation of grain boundary structure with controlled impurity distribution, and (3) achievement of high density (92.0% or more area proportion of main phase). This integration of multiple objectives into a single process dramatically improves productivity while maintaining excellent magnetic properties

Inventive Principle:
Principle #5Merging (Combining)

Data Source

PatentUS20230025223A1R-t-b based permanent magnet
Publication Date: 2023.01.26 TDK CORP
  • US20230025223A1 patent drawing
  • US20230025223A1 patent drawing
  • US20230025223A1 patent drawing

AI summary

An R-T-B based permanent magnet including R2T14B main phase crystal grains and a grain boundary. R represents one or more rare earth elements, T represents one or more iron group elements essentially including Fe or Fe and Co, and B represents boron. In a cross-section parallel to the alignment direction of the R-T-B based permanent magnet, the coverage of the R2T14B main phase crystal grains is 50.0% or more, and the area ratio of the R2T14B main phase crystal grains is 92.0% or more.