R-T-Cu-Mn-B Sintered Magnet Coercivity via Cu and Mn

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Solution Overview

Problem

The challenge lies in increasing the coercivity of rare-earth-transition metal-boron (R-T-B) based sintered magnets while minimizing the use of expensive and rare rare-earth elements like Dy and Tb, and overcoming limitations in adding Cu, which affects remanence and coercivity due to surface energy and grain boundary phase issues.

Innovation Solution

An R-T-Cu-Mn-B based sintered magnet composition is developed, with specific ranges for R, Cu, and Mn, including a higher percentage of Cu and Mn to enhance coercivity, where Cu forms interfacial films and Mn stabilizes the main phase, allowing for increased Cu addition without decomposing the R2T14B compound, even with reduced crystal grain size.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If Dy or Tb is added to increase coercivity, then coercivity is improved, but cost increases and main phase formation is interfered with

Engineering Contradiction:
ImprovecoercivityVSAvoidamount of Dy or Tb
Core Design Contradiction:
StrengthVSQuantity of substance

Solution Approach 1:

The patent replaces expensive rare-earth elements (Dy, Tb) with cheaper transition metal elements (Cu, Mn, Co) to achieve the same coercivity enhancement. Cu and Mn act as substitutes that provide similar magnetic strengthening effects without the high cost and formation interference issues associated with Dy and Tb.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The patent changes the compositional parameters by introducing specific ratios of Cu (0.01-0.5 at%) and Mn (0.01-0.5 at%) along with Co (0.1-5 at%) to modify the magnetic properties. This parameter adjustment allows achieving high coercivity through transition metal addition rather than relying on expensive rare-earth elements.

Inventive Principle:
Principle #35Parameter changes

2Strength

If Cu is added to increase coercivity, then coercivity is improved, but remanence decreases

Engineering Contradiction:
ImprovecoercivityVSAvoidremanence
Core Design Contradiction:
StrengthVSStability of the object's composition

Solution Approach 1:

The patent combines Cu and Mn in specific ratios (Cu: 0.01-0.5 at%, Mn: 0.01-0.5 at%) to achieve synergistic effects. The combination allows Cu to enhance coercivity while Mn helps maintain remanence by stabilizing the main phase and preventing excessive Cu-induced degradation.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent creates a composite alloy system R-T-Cu-Mn-B that integrates multiple elements with complementary functions. The composite structure leverages Cu for coercivity enhancement, Mn for remanence maintenance, and Co for overall magnetic property optimization, achieving balanced performance.

Inventive Principle:
Principle #40Composite materials

3Strength

If crystal grain size is reduced to increase coercivity, then coercivity is improved, but interface between main and grain boundary phases increases

Engineering Contradiction:
ImprovecoercivityVSAvoidinterface area
Core Design Contradiction:
StrengthVSArea of stationary object

Solution Approach 1:

The patent introduces transition metal elements (Cu, Mn, Co) as intermediary substances that preferentially locate at the grain boundary interfaces. These intermediaries improve the quality and magnetic properties of the grain boundary phase, allowing fine grain structures to maintain good interfacial characteristics and achieve high coercivity without excessive interface degradation.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly increases coercivity and maintains remanence, providing improved thermal resistance and magnetization stability, enabling the use of these magnets in applications like motors.

Implementation Method 1

Cu would be distributed in the form of a film over the interface between the main phase and the grain boundary phase and eliminate microscopic defect surrounding the main phase

Methodology Applied
Scientific EffectFilm formation: Thin Films

Implementation Method 2

Mn stabilizes the main phase, allowing for increased Cu addition without decomposing the R2T14B compound

Methodology Applied
Scientific EffectPhase stabilization:

Implementation Method 3

a sintered magnet obtained from a compacted powder

Methodology Applied
Scientific EffectSintering: Sintering

Data Source

PatentEP2302646B1R-t-cu-mn-b type sintered magnet
Publication Date: 2018.10.31 PROTERIAL LTD
  • EP2302646B1 patent drawingFigure 1
  • EP2302646B1 patent drawingFigure 2

AI summary

An R-T-Cu-Mn-B based sintered magnet includes: 12.0 at% to 15.0 at% of R, which is at least one of the rare-earth elements that include Y and of which at least 50 at% is Pr and/or Nd; 5.5 at% to 6.5 at% of B; 0.08 at% to 0.35 at% of Cu; 0.04 at% to less than 0.2 at% of Mn; at most 2 at% (including 0 at%) of M, which is one, two, or more elements that are selected from the group consisting of Al, Ti, V, Cr, Ni, Zn, Ga, Zr, Nb, Mo, Ag, In, Sn, Hf, Ta, W, Au, Pb and Bi; and T as the balance, which is either Fe alone or Fe and Co and of which at most 20 at% is Co if T includes both Fe and Co.