RTX Intermetallic Catalyst for Ammonia Synthesis

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Solution Overview

Problem

Intermetallic compounds used as catalysts for ammonia synthesis are prone to decomposition into nitrides at reaction temperatures, leading to poor stability and catalytic activity.

Innovation Solution

A ternary intermetallic compound represented by RTX, where R is a lanthanoid element, T is a transition metal, and X is Si, Al, or Ge, with a transition metal M supported on it, exhibiting improved ammonia synthesis activity and stability at lower temperatures.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If intermetallic compounds are used as catalysts for ammonia synthesis, then catalytic activity is improved, but stability deteriorates due to decomposition into nitrides at reaction temperatures

Engineering Contradiction:
Improveammonia synthesis activityVSAvoidcatalyst stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The invention uses a composite catalyst system comprising an intermetallic compound (such as CeFe2, CeCo2, CeRu2, LaFe2, LaCo2, or LaRu2) combined with a transition metal (Fe, Co, or Ru). This composite structure allows the intermetallic compound to provide high catalytic activity while the transition metal component maintains structural stability and prevents decomposition into nitrides at reaction temperatures, thereby resolving the contradiction between activity and stability.

Inventive Principle:
Principle #40Composite materials

2Use of energy by stationary object

If reaction temperature is reduced below Haber-Bosch conditions, then energy consumption is reduced, but catalytic activity deteriorates

Engineering Contradiction:
Improveenergy consumptionVSAvoidammonia synthesis activity
Core Design Contradiction:
Use of energy by stationary objectVSProductivity

Solution Approach 1:

The invention changes the chemical composition parameters of the catalyst from conventional iron-based or ruthenium-based catalysts to intermetallic compounds combined with transition metals. This parameter change enables the catalyst to maintain high activity at lower temperatures (200-400°C), thus reducing energy consumption while preserving productivity. The intermetallic structure provides unique electronic and geometric properties that facilitate nitrogen activation at lower temperatures.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If conventional iron-based catalysts are used, then stability is maintained, but energy consumption increases due to high temperature requirements

Engineering Contradiction:
Improvecatalyst stabilityVSAvoidenergy consumption
Core Design Contradiction:
ReliabilityVSUse of energy by stationary object

Solution Approach 1:

The invention changes the catalyst composition from conventional iron-based materials to intermetallic compounds (CeFe2, CeCo2, CeRu2, LaFe2, LaCo2, LaRu2) combined with transition metals. This parameter change enables operation at lower temperatures (200-400°C versus 400-500°C for conventional catalysts), reducing energy consumption while the transition metal component ensures stability is maintained.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The transition metal-supported intermetallic compound demonstrates enhanced hydrogen storage and release properties, along with increased ammonia synthesis activity and stability, making it suitable for ammonia synthesis and hydrogenation reactions.

Implementation Method 1

the intermetallic compound which has stored hydrogen can be used for hydrogenation reaction of other compounds

Methodology Applied
Scientific EffectHydrogen storage: Absorption (physical)

Implementation Method 2

the intermetallic compound-hydrogen complex...is capable of releasing hydrogen at 400°C or less

Methodology Applied
Scientific EffectHydrogen release: Desorption

Implementation Method 3

a catalyst comprising the transition metal-supported intermetallic compound...a method for producing ammonia, comprising contacting nitrogen and hydrogen with a catalyst

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP3653296B1Intermetallic compound, hydrogen storage/release material, catalyst and method for producing ammonia
Publication Date: 2023.12.13 THE JAPAN SCI & TECH AGENCY
  • EP3653296B1 patent drawingFigure 1~2
  • EP3653296B1 patent drawingFigure 3
  • EP3653296B1 patent drawingFigure 4(a)~4(b)

AI summary

Provided are an intermetallic compound having high stability and high activity, and a catalyst using the same. A hydrogen storage/release material containing an intermetallic compound represented by formula (1): RTX ... (1) wherein R represents a lanthanoid element, T represents a transition metal in period 4 or period 5 in the periodic table, and X represents Si, Al or Ge.