Rubber Composition Dry-Mixing Masterbatches

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Solution Overview

Problem

Existing rubber compositions used for pneumatic tires, particularly those involving the mixing of rubber wet masterbatches, face challenges in achieving low exothermic performance and high rubber hardness, as the homogenization process limits the formation of specific structures that enhance these properties.

Innovation Solution

A rubber composition is developed by dry-mixing rubber wet masterbatch A with a high nitrogen adsorption specific surface area carbon black and rubber wet masterbatch B with a low nitrogen adsorption specific surface area carbon black, at specific content ratios, to create a sea-island structure that improves vulcanized rubber's low exothermic performance and rubber hardness.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If rubber wet masterbatches are mixed and dried to achieve homogeneity, then the composition becomes uniform throughout the system, but the low exothermic performance and rubber hardness are not improved

Engineering Contradiction:
Improvehomogeneity of compositionVSAvoidexothermic performance
Core Design Contradiction:
Stability of the object's compositionVSTemperature

Solution Approach 1:

The invention applies local quality by creating a sea-island structure where different rubber phases with distinct properties are distributed throughout the material. The continuous phase (sea) and dispersed phase (island) each have different compositions and properties, allowing local regions to contribute differently to overall performance, particularly enabling low exothermic performance while maintaining structural integrity

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The invention uses composite materials by combining two different rubber wet masterbatches (A and B) with different carbon black contents to form a multi-phase system. This composite structure allows the material to exhibit properties that neither phase alone could achieve, specifically achieving both low exothermic performance and high rubber hardness through the synergistic interaction of the sea and island phases

Inventive Principle:
Principle #40Composite materials

2Stability of the object's composition

If rubber wet masterbatches are mixed and dried to achieve homogeneity, then the composition becomes uniform throughout the system, but the rubber hardness is not easily heightened

Engineering Contradiction:
Improvehomogeneity of compositionVSAvoidrubber hardness
Core Design Contradiction:
Stability of the object's compositionVSStrength

Solution Approach 1:

The sea-island structure enables local quality enhancement where the dispersed island phases containing rubber wet masterbatch A (with higher carbon black content) are distributed within the continuous sea phase of rubber wet masterbatch B. This localized distribution of high carbon black regions provides enhanced rubber hardness while the overall composite maintains compositional stability

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

By forming a composite of two rubber wet masterbatches with different carbon black contents, the invention achieves rubber hardness enhancement through the reinforcing effect of the dispersed phase while maintaining the stability of the overall composition. The interaction between the sea and island phases creates a structure that resists deformation more effectively than a homogeneous mixture

Inventive Principle:
Principle #40Composite materials

3Temperature

If carbon blacks with different nitrogen adsorption specific surface areas are used in specific ratios, then low exothermic performance and rubber hardness are improved, but the mixing process becomes more complex

Engineering Contradiction:
Improvelow exothermic performanceVSAvoidmixing process complexity
Core Design Contradiction:
TemperatureVSDevice complexity

Solution Approach 1:

The invention applies preliminary action by pre-preparing two distinct rubber wet masterbatches (A and B) with specific carbon black contents and properties before combining them. This pre-preparation allows the final mixing step to be simpler while ensuring that the correct phases with appropriate properties are present in the correct proportions to achieve the desired sea-island structure and performance characteristics

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention uses parameter changes by controlling the nitrogen adsorption specific surface area (NA and NB) and carbon black content ratios (LA and LB) of the two rubber wet masterbatches. By adjusting these parameters within specific ranges and satisfying the inequality NA×LA−NB×LB≥1800, the invention achieves optimal low exothermic performance and rubber hardness while managing mixing process complexity through defined parameter relationships

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The resulting vulcanized rubber exhibits enhanced low exothermic performance and increased rubber hardness, achieving a balance between fuel efficiency and rigidity in pneumatic tires.

Implementation Method 1

a carbon black A having a nitrogen adsorption specific surface area (N2SA) of NA (m2/g) and a carbon black B having a nitrogen adsorption specific surface area (N2SA) of NB (m2/g)

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentUS10017612B2Rubber composition
Publication Date: 2018.07.10 TOYO TIRE CORP

AI summary

A rubber composition obtained by dry-mixing a rubber wet masterbatch A containing a carbon black A having a nitrogen adsorption specific: surface area (N2SA) of NA (m2/g) with a rubber wet masterbatch B containing a carbon black B having a nitrogen adsorption specific surface area (N2SA) of NB (m2/g),wherein the content ratio of the rubber wet masterbatch A to the rubber wet masterbatch B is from 5/95 to 40/60, andwhen the content proportion of the carbon black A in the rubber wet masterbatch A is represented by LA, and that of the carbon black B in the rubber wet masterbatch B is represented by LB, the specific expressions are satisfied.