Rubber Composition Mixing Sequence for Wet Grip

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Solution Overview

Problem

Existing rubber compositions used in pneumatic tires, particularly those with high styrene-butadiene rubber content, face challenges in balancing wet grip performance, low temperature performance, abrasion resistance, and low heat generation (rolling resistance) due to the compatibility of syndiotactic-1,2-polybutadiene (SPB) with silica, which hinders the effective exhibition of SPB's performance.

Innovation Solution

A method involving the initial kneading of diene rubber with silica, followed by the addition and kneading of SPB, to accelerate phase separation and enhance the wet grip performance while maintaining low temperature and abrasion resistance, involves adding 20 parts by mass or more of silica to 100 parts by mass of diene rubber and then adding 3 to 20 parts by mass of SPB to the kneaded mixture.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If syndiotactic-1,2-polybutadiene (SPB) is added to diene rubber together with silica or after silica addition, then processability and low rolling resistance are improved, but wet grip performance deteriorates due to compatibility between SPB and silica

Engineering Contradiction:
ImproveprocessabilityVSAvoidwet grip performance
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent divides the mixing process into two distinct stages: first mixing diene rubber with silica to form a master batch, then separately adding SPB in a second mixing stage. This segmentation prevents SPB from directly contacting and interacting with silica, thereby avoiding the compatibility issue that would otherwise reduce wet grip performance while still achieving improved processability and low rolling resistance.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent performs preliminary mixing of diene rubber with silica to create a master batch before adding SPB. This preliminary action ensures that silica is already uniformly distributed in the diene rubber matrix, and when SPB is subsequently added, it does not directly interact with silica particles, thus preserving the ice controlling action and wet grip performance while still achieving the desired processability improvements.

Inventive Principle:
Principle #10Preliminary action

2Reliability

If high styrene content is used in styrene-butadiene rubber to improve wet grip performance, then grip performance on wet road surface is improved, but low temperature performance, abrasion resistance, and low heat generation performance deteriorate

Engineering Contradiction:
Improvewet grip performanceVSAvoidlow temperature performance, abrasion resistance, low heat generation performance
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The patent creates a composite rubber composition by combining diene rubber (such as SBR with optimized styrene content) with syndiotactic-1,2-polybutadiene (SPB) as a functional additive. This composite approach allows the base diene rubber to provide good wet grip performance while SPB contributes ice controlling action and maintains low temperature flexibility, thereby achieving a balance among wet grip performance, low temperature performance, abrasion resistance, and low heat generation performance without requiring excessively high styrene content.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively brings out the performance of SPB, improving wet grip performance and maintaining low temperature and abrasion resistance, while suppressing the deterioration of low heat generation performance, by controlling the mixing and phase separation of silica and SPB within the rubber composition.

Implementation Method 1

kneading 20 parts by mass or more of silica with 100 parts by mass of diene rubber

Methodology Applied
Scientific EffectMechanical mixing:

Implementation Method 2

adding from 3 to 20 parts by mass of syndiotactic-1,2-polybutadiene to the kneaded mixture obtained, followed by kneading... to accelerate phase separation

Methodology Applied
Scientific EffectPhase separation:

Data Source

PatentUS9796818B2Method for producing rubber composition
Publication Date: 2017.10.24 TOYO TIRE CORP

AI summary

A method for producing a rubber composition, which comprises kneading 20 parts by mass or more of silica with 100 parts by mass of diene rubber, and adding from 3 to 20 parts by mass of syndiotactic-1,2-polybutadiene to the kneaded mixture obtained, followed by kneading is disclosed. This method brings out characteristics of syndiotactic-1,2-polybutadiene and can improve wet grip performance.